2-(1-hydroxy-5,8-dimethyl-1,2,3,4-tetrahydro-[2]naphthyl)-propionic acid-lactone

Base Information

Chemical Name:2-(1-hydroxy-5,8-dimethyl-1,2,3,4-tetrahydro-[2]naphthyl)-propionic acid-lactone
CAS No.:96933-90-3
Molecular Formula:C₁₅H₁₈O₂
Molecular Weight:230.307
Hs Code.:

Synonyms:2-(1-hydroxy-5,8-dimethyl-1,2,3,4-tetrahydro-[2]naphthyl)-propionic acid-lactone

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Chemical Property of 2-(1-hydroxy-5,8-dimethyl-1,2,3,4-tetrahydro-[2]naphthyl)-propionic acid-lactone

Chemical Property:

Purity/Quality:

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Technology Process of 2-(1-hydroxy-5,8-dimethyl-1,2,3,4-tetrahydro-[2]naphthyl)-propionic acid-lactone

There total 3 articles about 2-(1-hydroxy-5,8-dimethyl-1,2,3,4-tetrahydro-[2]naphthyl)-propionic acid-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 478-59-1
isohyposantonin

: 478-58-0,478-59-1,96933-90-3,108511-37-1,108511-39-3
(3R,3aR,9bR)-3,6,9-Trimethyl-3a,4,5,9b-tetrahydro-3H-naphtho[1,2-b]furan-2-one

Guidance literature:: With potassium carbonate; In xylene; for 72h; Heating;
DOI:10.1021/jo00389a045

Reference yield:

: 478-58-0
hyposantonin

: 478-58-0,478-59-1,96933-90-3,108511-37-1,108511-39-3
(3R,3aR,9bR)-3,6,9-Trimethyl-3a,4,5,9b-tetrahydro-3H-naphtho[1,2-b]furan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / 10percent aq. KOH / ethanol / 2.5 h / Heating

2: 0.035 g / K₂CO₃ / xylene / 72 h / Heating

With potassium hydroxide; potassium carbonate; In ethanol; xylene;
DOI:10.1021/jo00389a045

Reference yield:

: 481-06-1
santonin

: 478-58-0,478-59-1,96933-90-3,108511-37-1,108511-39-3
(3R,3aR,9bR)-3,6,9-Trimethyl-3a,4,5,9b-tetrahydro-3H-naphtho[1,2-b]furan-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: CeCl₃*7H₂O, NaBH₄ / methanol / 0.67 h / 0 °C

2: 58 percent / 10percent aq. KOH / ethanol / 2.5 h / Heating

3: 0.035 g / K₂CO₃ / xylene / 72 h / Heating

With potassium hydroxide; sodium tetrahydroborate; cerium(III) chloride; potassium carbonate; In methanol; ethanol; xylene;
DOI:10.1021/jo00389a045