Technology Process of C27H35Cl2N5O3
There total 5 articles about C27H35Cl2N5O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Dess-Martin periodane / dichloromethane / 20 °C
2: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C
3: 20 °C / Acidic conditions
4: potassium carbonate / acetone / Reflux
With
sodium tris(acetoxy)borohydride; potassium carbonate; Dess-Martin periodane;
In
dichloromethane; acetone;
1: Dess-Martin oxidation;
DOI:10.1016/j.bmcl.2012.04.118
- Guidance literature:
-
Multi-step reaction with 5 steps
1: chloroform / 20 °C
2: trifluoroacetic acid / dichloromethane / 20 °C
3: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C
4: 20 °C / Acidic conditions
5: potassium carbonate / acetone / Reflux
With
sodium tris(acetoxy)borohydride; potassium carbonate; trifluoroacetic acid;
In
dichloromethane; chloroform; acetone;
DOI:10.1016/j.bmcl.2012.04.118
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trifluoroacetic acid / dichloromethane / 20 °C
2: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C
3: 20 °C / Acidic conditions
4: potassium carbonate / acetone / Reflux
With
sodium tris(acetoxy)borohydride; potassium carbonate; trifluoroacetic acid;
In
dichloromethane; acetone;
DOI:10.1016/j.bmcl.2012.04.118