C₆₉H₈₆N₂O₂S₂

Base Information

Chemical Name:C₆₉H₈₆N₂O₂S₂
CAS No.:1631755-10-6
Molecular Formula:C₆₉H₈₆N₂O₂S₂
Molecular Weight:1039.59
Hs Code.:

C<sub>69</sub>H<sub>86</sub>N<sub>2</sub>O<sub>2</sub>S<sub>2</sub>

Synonyms:C₆₉H₈₆N₂O₂S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₉H₈₆N₂O₂S₂

Chemical Property:

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Technology Process of C₆₉H₈₆N₂O₂S₂

There total 3 articles about C₆₉H₈₆N₂O₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.6%

: 1631755-15-1
9-hexyl-6-(3-(hexyloxy)phenyl)-N-(4-(hexyloxy)phenyl)-9H-carbazol-3-amine

: 1630989-35-3
C₂₇H₃₃BrS₂

: 1631755-10-6
C₆₉H₈₆N₂O₂S₂

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; XPhos; In toluene; Inert atmosphere; Reflux;
DOI:10.1021/ol5018036

Reference yield:

: 1631755-66-2
9-hexyl-3-(4-(hexyloxy)phenyl)-6-nitro-9H-carbazole

: 1631755-10-6
C₆₉H₈₆N₂O₂S₂

Guidance literature:: Multi-step reaction with 3 steps

1: palladium on activated charcoal; hydrogen / tetrahydrofuran / 20 °C

2: palladium diacetate; tri-tert-butyl phosphine; potassium tert-butylate / 1,2-dimethoxyethane / Inert atmosphere; Reflux

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; sodium t-butanolate / toluene / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; palladium on activated charcoal; potassium tert-butylate; hydrogen; palladium diacetate; sodium t-butanolate; XPhos; In tetrahydrofuran; 1,2-dimethoxyethane; toluene; 3: |Buchwald-Hartwig Coupling;
DOI:10.1021/ol5018036

Reference yield:

: 921937-76-0
2-(4-(hexyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1631755-10-6
C₆₉H₈₆N₂O₂S₂

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane / Inert atmosphere; Reflux

2: palladium on activated charcoal; hydrogen / tetrahydrofuran / 20 °C

3: palladium diacetate; tri-tert-butyl phosphine; potassium tert-butylate / 1,2-dimethoxyethane / Inert atmosphere; Reflux

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; sodium t-butanolate / toluene / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium on activated charcoal; potassium tert-butylate; hydrogen; palladium diacetate; potassium carbonate; sodium t-butanolate; XPhos; In tetrahydrofuran; 1,2-dimethoxyethane; toluene; 1: |Suzuki Coupling / 4: |Buchwald-Hartwig Coupling;
DOI:10.1021/ol5018036