1-(1-propyl)-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

Base Information

Chemical Name:1-(1-propyl)-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole
CAS No.:917247-75-7
Molecular Formula:C₃₇H₃₆Cl₃NO₄
Molecular Weight:665.056
Hs Code.:

Synonyms:1-(1-propyl)-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

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Chemical Property of 1-(1-propyl)-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

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Technology Process of 1-(1-propyl)-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

There total 4 articles about 1-(1-propyl)-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 917247-73-5
3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

: 107-08-4
1-iodo-propane

: 917247-75-7
1-(1-propyl)-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.333333h;
DOI:10.1080/15257770500265646

Reference yield:

: 917247-69-9
1-acetyl-2,5,6-trichloroindole

: 917247-75-7
1-(1-propyl)-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / BF₃*Et₂O / CH₂Cl₂ / 0.17 h / 0 °C

2: 99 percent / MeNH₂ / methanol / 0.5 h / 20 °C

3: 100 percent / NaH / tetrahydrofuran; various solvent(s) / 0.33 h / 0 - 20 °C

With boron trifluoride diethyl etherate; sodium hydride; methylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1080/15257770500265646

Reference yield:

: 917247-71-3
1-acetyl-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

: 917247-75-7
1-(1-propyl)-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / MeNH₂ / methanol / 0.5 h / 20 °C

2: 100 percent / NaH / tetrahydrofuran; various solvent(s) / 0.33 h / 0 - 20 °C

With sodium hydride; methylamine; In tetrahydrofuran; methanol;
DOI:10.1080/15257770500265646