(Sp)-ethyl 3-(2-(((((S)-1-ethoxy-1-oxopropan-2-yl)amino)(4-(methylsulfonyl)phenoxy)phosphoryl)oxy)phenyl)propanoate

Base Information

Chemical Name:(Sp)-ethyl 3-(2-(((((S)-1-ethoxy-1-oxopropan-2-yl)amino)(4-(methylsulfonyl)phenoxy)phosphoryl)oxy)phenyl)propanoate
CAS No.:1412427-17-8
Molecular Formula:C₂₃H₃₀NO₉PS
Molecular Weight:527.532
Hs Code.:

Synonyms:(Sp)-ethyl 3-(2-(((((S)-1-ethoxy-1-oxopropan-2-yl)amino)(4-(methylsulfonyl)phenoxy)phosphoryl)oxy)phenyl)propanoate

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Chemical Property of (Sp)-ethyl 3-(2-(((((S)-1-ethoxy-1-oxopropan-2-yl)amino)(4-(methylsulfonyl)phenoxy)phosphoryl)oxy)phenyl)propanoate

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Technology Process of (Sp)-ethyl 3-(2-(((((S)-1-ethoxy-1-oxopropan-2-yl)amino)(4-(methylsulfonyl)phenoxy)phosphoryl)oxy)phenyl)propanoate

There total 4 articles about (Sp)-ethyl 3-(2-(((((S)-1-ethoxy-1-oxopropan-2-yl)amino)(4-(methylsulfonyl)phenoxy)phosphoryl)oxy)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20921-04-4
ethyl 3-(2-hydroxyphenyl)propanoate

: 1412427-17-8
(Sp)-ethyl 3-(2-(((((S)-1-ethoxy-1-oxopropan-2-yl)amino)(4-(methylsulfonyl)phenoxy)phosphoryl)oxy)phenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; trichlorophosphate / diethyl ether / 18 h / -78 - 20 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 7.33 h / -78 - 0 °C / Inert atmosphere

2.2: 12 h / -78 - 20 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

With triethylamine; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In diethyl ether; dichloromethane;

Reference yield:

: ethyl 3-(2-(((((S)-1-ethoxy-1-oxopropan-2-yl)amino)(4-(methylthio)phenoxy)phosphoryl)oxy)phenyl)propanoate

: 1412427-17-8
(Sp)-ethyl 3-(2-(((((S)-1-ethoxy-1-oxopropan-2-yl)amino)(4-(methylsulfonyl)phenoxy)phosphoryl)oxy)phenyl)propanoate

: 1412427-16-7
ethyl 3-(2-(((((S)-1-ethoxy-1-oxopropan-2-yl)amino)(4-(methylsulfonyl)phenoxy)phosphoryl)oxy)phenyl)propanoate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 12h; Inert atmosphere;

Reference yield:

: 119-84-6,1341-36-2
C₆H₄(CH₂CH₂C(O)O)

: 1412427-17-8
(Sp)-ethyl 3-(2-(((((S)-1-ethoxy-1-oxopropan-2-yl)amino)(4-(methylsulfonyl)phenoxy)phosphoryl)oxy)phenyl)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 12 h / 0 °C / Inert atmosphere

1.2: pH 6 - 6.5

2.1: triethylamine; trichlorophosphate / diethyl ether / 18 h / -78 - 20 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 7.33 h / -78 - 0 °C / Inert atmosphere

3.2: 12 h / -78 - 20 °C / Inert atmosphere

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

With sulfuric acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In diethyl ether; dichloromethane;