2-[3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]phenyl]ethanol

Base Information

Chemical Name:2-[3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]phenyl]ethanol
CAS No.:1222138-81-9
Molecular Formula:C₂₅H₂₆N₂O₄
Molecular Weight:418.492
Hs Code.:

Synonyms:2-[3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]phenyl]ethanol

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Chemical Property of 2-[3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]phenyl]ethanol

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Technology Process of 2-[3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]phenyl]ethanol

There total 1 articles about 2-[3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]phenyl]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 704914-05-6
3-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-5-(trimethylstannyl)pyridine

: 127201-31-4
2-(3-iodophenyl)ethan-1-ol

: 1222138-81-9
2-[3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]phenyl]ethanol

Guidance literature:: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride; In N,N-dimethyl-formamide; at 50 ℃; for 6h;

Reference yield:

: 1222138-81-9
2-[3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]phenyl]ethanol

: 1222134-87-3
2-[3-[5-[(2(S)-azetidinyl)methoxy]-3-pyridyl]phenyl]ethanol

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 2.16667h; under 750.075 Torr;

Reference yield:

: 1222138-81-9
2-[3-[5-[[1-(benzyloxycarbonyl)-2(S)-azetidinyl]methoxy]-3-pyridyl]phenyl]ethanol

: 2-[3-[5-[(2(S)-azetidinyl)methoxy]-3-pyridyl]phenyl]ethanol hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol; water / 2.17 h / 20 °C / Inert atmosphere

2: hydrogenchloride / methanol; water

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; In methanol; water;