Technology Process of methyl 3,4-di-O-benzoyl-2,6-dideoxyhexopyranoside
There total 9 articles about methyl 3,4-di-O-benzoyl-2,6-dideoxyhexopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
toluene;
at 95 ℃;
for 24h;
Inert atmosphere;
DOI:10.1021/acs.jnatprod.5b01051
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / 22 h / 0 - 20 °C / Inert atmosphere
2: N-Bromosuccinimide; barium carbonate / tetrachloromethane / 5 h / 90 °C / Inert atmosphere
3: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 24 h / 95 °C / Inert atmosphere
With
pyridine; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; barium carbonate;
In
tetrachloromethane; toluene;
DOI:10.1021/acs.jnatprod.5b01051
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-Bromosuccinimide; barium carbonate / tetrachloromethane / 5 h / 90 °C / Inert atmosphere
2: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 24 h / 95 °C / Inert atmosphere
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; barium carbonate;
In
tetrachloromethane; toluene;
DOI:10.1021/acs.jnatprod.5b01051
