3'-α-(selenophenyl)-2',3'-dideoxythymidine-5'-yl H-phosphonate triethylammonium salt

Base Information

Chemical Name:3'-α-(selenophenyl)-2',3'-dideoxythymidine-5'-yl H-phosphonate triethylammonium salt
CAS No.:1419743-18-2
Molecular Formula:C₆H₁₅N*C₁₆H₁₉N₂O₆PSe
Molecular Weight:546.462
Hs Code.:

Synonyms:3'-α-(selenophenyl)-2',3'-dideoxythymidine-5'-yl H-phosphonate triethylammonium salt

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Chemical Property of 3'-α-(selenophenyl)-2',3'-dideoxythymidine-5'-yl H-phosphonate triethylammonium salt

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Technology Process of 3'-α-(selenophenyl)-2',3'-dideoxythymidine-5'-yl H-phosphonate triethylammonium salt

There total 2 articles about 3'-α-(selenophenyl)-2',3'-dideoxythymidine-5'-yl H-phosphonate triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 131933-44-3
1-(2,3-dideoxy-3-C-selenophenyl-β-D-erythro-pentofuranosyl)thymine

: 121-44-8
triethylamine

: 1419743-18-2
3'-α-(selenophenyl)-2',3'-dideoxythymidine-5'-yl H-phosphonate triethylammonium salt

Guidance literature:: triethylamine; With 1H-imidazole; phosphorus trichloride; In dichloromethane; at -10 ℃; for 0.5h;

1-(2,3-dideoxy-3-C-selenophenyl-β-D-erythro-pentofuranosyl)thymine; In dichloromethane; at -10 ℃; for 2h;
DOI:10.1016/j.bmcl.2012.11.050

Reference yield:

: 131933-44-3
1-(2,3-dideoxy-3-C-selenophenyl-β-D-erythro-pentofuranosyl)thymine

: 1419743-18-2
3'-α-(selenophenyl)-2',3'-dideoxythymidine-5'-yl H-phosphonate triethylammonium salt

Guidance literature:: Multi-step reaction with 2 steps

1: pivaloyl chloride; pyridine / dichloromethane

2: acetonitrile

With pyridine; pivaloyl chloride; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2012.11.050