4-fluoro-2-phenylazoacetanilide

Base Information

Chemical Name:4-fluoro-2-phenylazoacetanilide
CAS No.:313485-91-5
Molecular Formula:C₁₄H₁₂FN₃O
Molecular Weight:257.267
Hs Code.:

Synonyms:4-fluoro-2-phenylazoacetanilide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-fluoro-2-phenylazoacetanilide

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Technology Process of 4-fluoro-2-phenylazoacetanilide

There total 1 articles about 4-fluoro-2-phenylazoacetanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 22380-13-8
N-acetyl-2-amino-4-fluoroaniline

: 586-96-9
Nitrosobenzene

: 313485-91-5
4-fluoro-2-phenylazoacetanilide

Guidance literature:: With acetic acid; In ethanol; at 25 ℃; for 15h;
DOI:10.1021/tx0000724

Reference yield: 94.0%

: 313485-91-5
4-fluoro-2-phenylazoacetanilide

: 313485-92-6
4-fluoro-2-phenylazoaniline

Guidance literature:: With potassium hydroxide; In methanol; for 15h; Heating;
DOI:10.1021/tx0000724

Reference yield:

: 313485-91-5
4-fluoro-2-phenylazoacetanilide

: (4-fluoro-2-phenylazo-phenyl)-methyl-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / KOH / methanol / 15 h / Heating

2: 31 percent / AcOH; aq. HCl / 0.25 h / 80 °C

3: 55 percent / methanol / 12 h / 50 °C

4: 82 percent / aq. NaOH / methanol / 5 h / 20 °C

With hydrogenchloride; potassium hydroxide; sodium hydroxide; acetic acid; In methanol;
DOI:10.1021/tx0000724