Thiophosphoric acid S-octadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Base Information

Chemical Name:Thiophosphoric acid S-octadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester
CAS No.:143599-64-8
Molecular Formula:C₅₉H₇₉O₈PS
Molecular Weight:979.311
Hs Code.:

Synonyms:Thiophosphoric acid S-octadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

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Chemical Property of Thiophosphoric acid S-octadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

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Technology Process of Thiophosphoric acid S-octadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

There total 3 articles about Thiophosphoric acid S-octadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2885-00-9
Octadecanethiol

: 143599-64-8
Thiophosphoric acid S-octadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) n-BuLi / 1) THF, 0 deg C, 30 min, 2) room temp., 1 h

2: CH₂Cl₂ / 6 h / Ambient temperature

3: triisopropylbenzenesulfonyl chloride (TPSCl), NEt₃, pyridine / 24 h / Ambient temperature

With pyridine; n-butyllithium; triisopropylbenzenesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)74812-X

Reference yield:

: 143570-22-3
Thiophosphoric acid O,O'-diethyl ester S-octadecyl ester

: 143599-64-8
Thiophosphoric acid S-octadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 6 h / Ambient temperature

2: triisopropylbenzenesulfonyl chloride (TPSCl), NEt₃, pyridine / 24 h / Ambient temperature

With pyridine; triisopropylbenzenesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)74812-X

Reference yield:

: 128371-67-5
C₂₄H₅₅O₃PSSi₂

: 6195-45-5,13264-84-1,22132-86-1,25018-91-1,26277-05-4,28366-79-2,30694-52-1
DL-2,3,4,5,6-penta-O-benzyl-myo-inositol

: 143599-64-8
Thiophosphoric acid S-octadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Guidance literature:: With pyridine; triisopropylbenzenesulfonyl chloride; triethylamine; for 24h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4039(00)74812-X