Technology Process of C28H45NOSSn
There total 6 articles about C28H45NOSSn which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); triethylamine;
at 120 ℃;
for 0.333333h;
Inert atmosphere;
Microwave irradiation;
DOI:10.1016/j.bmcl.2012.11.043
- Guidance literature:
-
Multi-step reaction with 5 steps
1: copper(l) iodide; potassium carbonate / isopropyl alcohol; ethylene glycol / 68 h / 20 - 80 °C / Inert atmosphere
2: thionyl chloride; N,N-dimethyl-formamide / 3 h / 85 °C / Inert atmosphere
3: thionyl chloride; N,N-dimethyl-formamide / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere
4: borane-THF / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere; Reflux
5: tetrakis(triphenylphosphine) palladium(0); triethylamine / 0.33 h / 120 °C / Inert atmosphere; Microwave irradiation
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); thionyl chloride; borane-THF; potassium carbonate; triethylamine; N,N-dimethyl-formamide;
In
tetrahydrofuran; ethylene glycol; isopropyl alcohol;
DOI:10.1016/j.bmcl.2012.11.043
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride; N,N-dimethyl-formamide / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere
2: borane-THF / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere; Reflux
3: tetrakis(triphenylphosphine) palladium(0); triethylamine / 0.33 h / 120 °C / Inert atmosphere; Microwave irradiation
With
tetrakis(triphenylphosphine) palladium(0); thionyl chloride; borane-THF; triethylamine; N,N-dimethyl-formamide;
In
tetrahydrofuran;
DOI:10.1016/j.bmcl.2012.11.043
