2-trimethylsilanyl-ethanesulfonic acid [2-bromo-4-(2-trimethylsilanyl-ethanesulfonylamino)-phenyl]-amide

Base Information

Chemical Name:2-trimethylsilanyl-ethanesulfonic acid [2-bromo-4-(2-trimethylsilanyl-ethanesulfonylamino)-phenyl]-amide
CAS No.:487047-44-9
Molecular Formula:C₁₆H₃₁BrN₂O₄S₂Si₂
Molecular Weight:515.64
Hs Code.:

Synonyms:2-trimethylsilanyl-ethanesulfonic acid [2-bromo-4-(2-trimethylsilanyl-ethanesulfonylamino)-phenyl]-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-trimethylsilanyl-ethanesulfonic acid [2-bromo-4-(2-trimethylsilanyl-ethanesulfonylamino)-phenyl]-amide

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Technology Process of 2-trimethylsilanyl-ethanesulfonic acid [2-bromo-4-(2-trimethylsilanyl-ethanesulfonylamino)-phenyl]-amide

There total 1 articles about 2-trimethylsilanyl-ethanesulfonic acid [2-bromo-4-(2-trimethylsilanyl-ethanesulfonylamino)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 13296-69-0
2-bromo-p-phenylenediamine

: 106018-85-3
2-trimethylsilanyl-ethanesulfonyl chloride

: 487047-44-9
2-trimethylsilanyl-ethanesulfonic acid [2-bromo-4-(2-trimethylsilanyl-ethanesulfonylamino)-phenyl]-amide

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1021/ol026849x

Reference yield:

: (E)-4-Tributylstannanyl-but-3-enoic acid methyl ester

: 487047-44-9
2-trimethylsilanyl-ethanesulfonic acid [2-bromo-4-(2-trimethylsilanyl-ethanesulfonylamino)-phenyl]-amide

: (Z)-4-[2,5-Bis-(2-trimethylsilanyl-ethanesulfonylamino)-phenyl]-but-3-enoic acid methyl ester

: (E)-4-[2,5-Bis-(2-trimethylsilanyl-ethanesulfonylamino)-phenyl]-but-3-enoic acid methyl ester

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-4-methyl-phenol; In toluene; for 12h; Title compound not separated from byproducts.; Heating;
DOI:10.1021/ol026849x