N-[2-(4-amino-phenyl)-ethyl]-N-[2-(naphthalen-1-yloxy)-ethyl]-acetamide

Base Information

Chemical Name:N-[2-(4-amino-phenyl)-ethyl]-N-[2-(naphthalen-1-yloxy)-ethyl]-acetamide
CAS No.:860616-34-8
Molecular Formula:C₂₂H₂₄N₂O₂
Molecular Weight:348.445
Hs Code.:

<i>N</i>-[2-(4-amino-phenyl)-ethyl]-<i>N</i>-[2-(naphthalen-1-yloxy)-ethyl]-acetamide

Synonyms:N-[2-(4-amino-phenyl)-ethyl]-N-[2-(naphthalen-1-yloxy)-ethyl]-acetamide

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Chemical Property of N-[2-(4-amino-phenyl)-ethyl]-N-[2-(naphthalen-1-yloxy)-ethyl]-acetamide

Chemical Property:

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Technology Process of N-[2-(4-amino-phenyl)-ethyl]-N-[2-(naphthalen-1-yloxy)-ethyl]-acetamide

There total 8 articles about N-[2-(4-amino-phenyl)-ethyl]-N-[2-(naphthalen-1-yloxy)-ethyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6270-07-1
N-<2-(4-nitrophenyl)ethyl>acetamide

: 860616-34-8
N-[2-(4-amino-phenyl)-ethyl]-N-[2-(naphthalen-1-yloxy)-ethyl]-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / 47percent HBr / 6 h / Heating

2: K₂CO₃ / acetonitrile / 20 °C

3: K₂CO₃ / acetonitrile / Heating

4: aq. HCl; iron; ammonium chloride / acetone / 45 °C

With hydrogenchloride; ammonium chloride; iron; potassium carbonate; In acetone; acetonitrile;
DOI:10.1021/jm010574u

Reference yield:

: 446877-71-0
N-acetyl-N-[2-(naphth-1-yl-oxy)ethyl]-p-nitrophenethylamine

: 860616-34-8
N-[2-(4-amino-phenyl)-ethyl]-N-[2-(naphthalen-1-yloxy)-ethyl]-acetamide

Guidance literature:: With hydrogenchloride; ammonium chloride; iron; In acetone; at 45 ℃;
DOI:10.1021/jm010574u

Reference yield:

: 90-15-3
α-naphthol

: 860616-34-8
N-[2-(4-amino-phenyl)-ethyl]-N-[2-(naphthalen-1-yloxy)-ethyl]-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaOH; TBA / ethanol / 0.25 h / Heating

1.2: 47.4 percent / ethanol / 24 h / Heating

2.1: K₂CO₃ / acetonitrile / 20 °C

3.1: K₂CO₃ / acetonitrile / Heating

4.1: aq. HCl; iron; ammonium chloride / acetone / 45 °C

With hydrogenchloride; sodium hydroxide; ammonium chloride; iron; potassium carbonate; tert-butylamine; In ethanol; acetone; acetonitrile;
DOI:10.1021/jm010574u