methyl 2,2-dioxo-2λ-[1,2,3]oxatetrahydrothiazole-3-N-tert-butoxycarbonyl-4-carboxylate

Base Information

Chemical Name:methyl 2,2-dioxo-2λ-[1,2,3]oxatetrahydrothiazole-3-N-tert-butoxycarbonyl-4-carboxylate
CAS No.:913979-52-9
Molecular Formula:C₉H₁₅NO₇S
Molecular Weight:281.287
Hs Code.:

Synonyms:methyl 2,2-dioxo-2λ-[1,2,3]oxatetrahydrothiazole-3-N-tert-butoxycarbonyl-4-carboxylate

Suppliers and Price of methyl 2,2-dioxo-2λ-[1,2,3]oxatetrahydrothiazole-3-N-tert-butoxycarbonyl-4-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 4 raw suppliers

Chemical Property of methyl 2,2-dioxo-2λ-[1,2,3]oxatetrahydrothiazole-3-N-tert-butoxycarbonyl-4-carboxylate

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Technology Process of methyl 2,2-dioxo-2λ-[1,2,3]oxatetrahydrothiazole-3-N-tert-butoxycarbonyl-4-carboxylate

There total 3 articles about methyl 2,2-dioxo-2λ-[1,2,3]oxatetrahydrothiazole-3-N-tert-butoxycarbonyl-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.16%

: C₉H₁₅NO₆S

: 913979-52-9,1621706-89-5
methyl 2,2-dioxo-2λ-[1,2,3]oxatetrahydrothiazole-3-N-tert-butoxycarbonyl-4-carboxylate

Guidance literature:: With ruthenium trichloride; sodium periodate; In water; acetonitrile; at 0 - 20 ℃; for 4h;

Reference yield:

: 2766-43-0
N-tert-butyloxycarbonyl-L-serine methyl ester

: 913979-52-9,1621706-89-5
methyl 2,2-dioxo-2λ-[1,2,3]oxatetrahydrothiazole-3-N-tert-butoxycarbonyl-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; pyridine / acetonitrile / 3.5 h / -42 °C / Inert atmosphere

2: sodium periodate; ruthenium(III) trichloride hydrate / water; acetonitrile / 4.25 h / 0 - 20 °C

With pyridine; sodium periodate; thionyl chloride; ruthenium(III) trichloride hydrate; In water; acetonitrile;
DOI:10.1016/j.bmc.2014.07.023