AlMe₃(pyridine)

Base Information

Chemical Name:AlMe₃(pyridine)
CAS No.:6125-66-2
Molecular Formula:C₈H₁₄AlN
Molecular Weight:151.187
Hs Code.:

Synonyms:AlMe₃(pyridine)

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Chemical Property of AlMe₃(pyridine)

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Technology Process of AlMe₃(pyridine)

There total 5 articles about AlMe₃(pyridine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: tris(μ-ferrocene-1,1'-diyl)bis[(N-pyridine)aluminum]

: 97-93-8
triethylaluminum

: 102-54-5,55404-68-7
ferrocene

: 6125-66-2
AlMe₃(pyridine)

: [Fe(η5-C5H4)2]3Al3Et3

Guidance literature:: In hexane; dichloromethane-d2; (exclusion of air and moisture), suspn. of Al-Fe complex in CD2Cl2 cooled to -50°C treated with 2 equiv. of Et3Al in hexanes, stirred for30 min at room temp.; evapd.(vac.), washed (hexane);
DOI:10.1002/ejic.200900273

Reference yield: 46.0%

: 110-86-1
pyridine

: trimethylaluminium dimer

: 111795-33-6,111822-69-6,126911-86-2
(S)-3,3'-bis(triphenylsilyl)-2,2'-dihydroxy-1,1'-dinaphthyl

: 108-88-3,15644-74-3,16713-13-6
toluene

: 6125-66-2
AlMe₃(pyridine)

: 548476-04-6
Al(CH₃)(py)((S)-3,3'-bis(triphenylsilyl)-1,1'-bi-2,2'-naphthoxide))*C₆H₅CH₃

Guidance literature:: In toluene; benzene; using Schlenk techniques; to flask contg. benzene added soln. of AlMe3 in toluene; org. ligand dissolved in benzene slowly added to stirred mixt.; pyridine added; mixt. stirred for 17 h; evapd. to dryness; dissolved in toluene; layered with hexane; crystals were obtained; elem. anal.;
DOI:10.1021/om030011b

Reference yield:

: 110-86-1
pyridine

: [(C₅(CH₃)5)2Yb(Al(CH₃)3)2(SC₆H₅)]2

: 6125-66-2
AlMe₃(pyridine)

: [(C₅Me₅)2Yb(SC₆H₅)(pyridine)]

Guidance literature:: In ⁽²⁾H₈-toluene; addn. a few drops of pyridine to soln. of ((Me5C5)2Yb(AlMe3)2(SPh))2 in toluene-d8; monitoring by NMR;
DOI:10.1021/om020472h