benzyl N-chlorocarbamate

Base Information

• Chemical Name: benzyl N-chlorocarbamate
• CAS No.: 30830-47-8
• Molecular Formula: C₈H₈ClNO₂
• Molecular Weight: 185.61
• Mol file: 30830-47-8.mol

Synonyms:benzyl N-chlorocarbamate

Chemical Property of benzyl N-chlorocarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl N-chlorocarbamate

There total 2 articles about benzyl N-chlorocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

O-benzyl carbamate (621-84-1) → benzyl N-chlorocarbamate (30830-47-8)

Guidance literature:

With trichloroisocyanuric acid; In methanol; at 25 ℃; for 1h;

DOI:10.1002/chem.201503511

Reference yield: 3.0%

O-benzyl carbamate (621-84-1) → N,N-dichlorobenzyl carbamate (130867-23-1) + benzyl N-chlorocarbamate (30830-47-8)

Guidance literature:

With tert-butyl hypochloride; In d⁽⁴⁾-methanol; at 20 ℃; for 24h;

DOI:10.1021/jo8025737

Reference yield: 98.0%

5-nitro-quinoline-1-oxide (7613-19-6) + benzyl N-chlorocarbamate (30830-47-8) → 8-{[(benzyloxy)carbonyl]amino}-5-nitroquinoline-1-oxide

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver(I) acetate; silver(I) triflimide; In methanol; at 50 ℃; for 12h; under 760.051 Torr;

DOI:10.1002/chem.201503511

upstream raw materials:

O-benzyl carbamate

Downstream raw materials:

(2-Hydroxy-tetrahydro-pyran-3-yl)-carbamic acid benzyl ester

(2,2-Dimethoxy-cyclohexyl)-carbamic acid benzyl ester

(+/-)-2-cyclohexanone

(2-Ethoxy-2-methoxy-ethyl)-carbamic acid benzyl ester