N,N-dichlorobenzyl carbamate

Base Information

• Chemical Name: N,N-dichlorobenzyl carbamate
• CAS No.: 130867-23-1
• Molecular Formula: C₈H₇Cl₂NO₂
• Molecular Weight: 220.055

Synonyms:N,N-dichlorobenzyl carbamate

Chemical Property of N,N-dichlorobenzyl carbamate

Chemical Property:

Purity/Quality:

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Technology Process of N,N-dichlorobenzyl carbamate

There total 2 articles about N,N-dichlorobenzyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

O-benzyl carbamate (621-84-1) → N,N-dichlorobenzyl carbamate (130867-23-1)

Guidance literature:

With sodium hypochlorite; acetic acid; at 0 - 5 ℃; for 0.333333h;

DOI:10.1080/00397911.2010.488311

Reference yield: 3.0%

O-benzyl carbamate (621-84-1) → N,N-dichlorobenzyl carbamate (130867-23-1) + benzyl N-chlorocarbamate (30830-47-8)

Guidance literature:

With tert-butyl hypochloride; In d⁽⁴⁾-methanol; at 20 ℃; for 24h;

DOI:10.1021/jo8025737

Reference yield: 99.0%

N,N-dichlorobenzyl carbamate (130867-23-1) + (2-nitroethenyl)benzene (102-96-5) → benzyl (2,2-dichloro-2-nitro-1-phenylethyl)carbamate (1355707-55-9)

Guidance literature:

With potassium carbonate; In dichloromethane; at 20 ℃; for 8h; regioselective reaction;

DOI:10.1055/s-0030-1260245

upstream raw materials:

O-benzyl carbamate

Downstream raw materials:

benzyl [2,2-dichloro-1-(naphth-1-yl)-2-nitroethyl]carbamate

benzyl (2,2-dichloro-2-nitro-1-phenylethyl)carbamate

benzyl [2,2-dichloro-1-(4-fluorophenyl)-2-nitroethyl]carbamate

benzyl [2,2-dichloro-1-(3-chlorophenyl)-2-nitroethyl]carbamate

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