2-(4-Fluoro-phenyl)-1-[4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidin-1-yl]-ethanone

Base Information

Chemical Name:2-(4-Fluoro-phenyl)-1-[4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidin-1-yl]-ethanone
CAS No.:321547-45-9
Molecular Formula:C₃₀H₄₂FNO₄Si
Molecular Weight:527.752
Hs Code.:

Synonyms:2-(4-Fluoro-phenyl)-1-[4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidin-1-yl]-ethanone

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Chemical Property of 2-(4-Fluoro-phenyl)-1-[4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidin-1-yl]-ethanone

Chemical Property:

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Technology Process of 2-(4-Fluoro-phenyl)-1-[4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidin-1-yl]-ethanone

There total 2 articles about 2-(4-Fluoro-phenyl)-1-[4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidin-1-yl]-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 321547-57-3
4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidine

: 459-04-1
4-Fluorophenylacetyl chloride

: 321547-45-9
2-(4-Fluoro-phenyl)-1-[4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidin-1-yl]-ethanone

: 405-50-5
p-Fluorophenylacetic acid

Guidance literature:: With sodium hydroxide; In water; toluene; at 0 - 20 ℃; for 2.5h;

Reference yield:

: 321547-57-3
4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidine

: 321547-45-9
2-(4-Fluoro-phenyl)-1-[4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidin-1-yl]-ethanone

Guidance literature:: With hydrogenchloride; H₂; sodium hydroxide; sodium hydrogencarbonate; acetic acid; In hexane; water; ethyl acetate; toluene; 4-Fluorophenylacetyl chloride;

Reference yield:

: 321547-45-9
2-(4-Fluoro-phenyl)-1-[4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidin-1-yl]-ethanone

: {1-[2-(4-fluoro-phenyl)-ethyl]-piperidin-4-yl}-(2-methoxy-3-triisopropylsilanyloxy-phenyl)-methanol

Guidance literature:: 2-(4-Fluoro-phenyl)-1-[4-(2-methoxy-3-triisopropylsilanyloxy-benzoyl)-piperidin-1-yl]-ethanone; With dimethylsulfide borane complex; In toluene; at -38 - 20 ℃;

With methanol; In toluene; for 1h;