sodium (Z)-3-methoxycarbonyl-3-oxo-1-(4-trifluoromethyl)phenyl-propen-1-olate

Base Information

Chemical Name:sodium (Z)-3-methoxycarbonyl-3-oxo-1-(4-trifluoromethyl)phenyl-propen-1-olate
CAS No.:1383452-43-4
Molecular Formula:C₁₂H₈F₃O₄*Na
Molecular Weight:296.178
Hs Code.:

Synonyms:sodium (Z)-3-methoxycarbonyl-3-oxo-1-(4-trifluoromethyl)phenyl-propen-1-olate

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Chemical Property of sodium (Z)-3-methoxycarbonyl-3-oxo-1-(4-trifluoromethyl)phenyl-propen-1-olate

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Technology Process of sodium (Z)-3-methoxycarbonyl-3-oxo-1-(4-trifluoromethyl)phenyl-propen-1-olate

There total 1 articles about sodium (Z)-3-methoxycarbonyl-3-oxo-1-(4-trifluoromethyl)phenyl-propen-1-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 553-90-2
Dimethyl oxalate

: 709-63-7
1-(4-trifluoromethylphenyl)ethanone

: 1383452-43-4
sodium (Z)-3-methoxycarbonyl-3-oxo-1-(4-trifluoromethyl)phenyl-propen-1-olate

Guidance literature:: 1-(4-trifluoromethylphenyl)ethanone; With sodium methylate; In methanol; at 0 - 20 ℃; for 1h;

Dimethyl oxalate; In methanol; at 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2012.03.056

Reference yield: 63.0%

: 1383452-43-4
sodium (Z)-3-methoxycarbonyl-3-oxo-1-(4-trifluoromethyl)phenyl-propen-1-olate

: 302-15-8
methylhydrazine sulfuric acid

: 93618-49-6
methyl 1-methyl-3-[4-(trifluoromethyl)phenyl]-1H-pyrazole-5-carboxylate

: 1383452-44-5
1-methyl-5-[4-(trifluoromethyl)phenyl]-1Hpyrazole-3-carboxylate acid methyl ester

Guidance literature:: sodium (Z)-3-methoxycarbonyl-3-oxo-1-(4-trifluoromethyl)phenyl-propen-1-olate; methylhydrazine sulfuric acid; With acetic acid; at 105 ℃; for 1h; Inert atmosphere;

With sodium hydrogencarbonate; In ethanol;
DOI:10.1016/j.ejmech.2012.03.056

Reference yield:

: 1383452-43-4
sodium (Z)-3-methoxycarbonyl-3-oxo-1-(4-trifluoromethyl)phenyl-propen-1-olate

: 1383452-45-6
1-methyl-5-[4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 1 h / 105 °C / Inert atmosphere

2: hydrazine hydrate / methanol / 2 h / 100 °C / Inert atmosphere

With hydrazine hydrate; acetic acid; In methanol;
DOI:10.1016/j.ejmech.2012.03.056