C₄₁H₅₀O₅S₂

Base Information

• Chemical Name: C₄₁H₅₀O₅S₂
• CAS No.: 851178-78-4
• Molecular Formula: C₄₁H₅₀O₅S₂
• Molecular Weight: 686.977
• Mol file: 851178-78-4.mol

Synonyms:C₄₁H₅₀O₅S₂

Chemical Property of C₄₁H₅₀O₅S₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₄₁H₅₀O₅S₂

There total 1 articles about C₄₁H₅₀O₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

benzyl bromide (100-39-0) + (2R,3R,4S,5R)-5-Allyloxy-1,2,4-tris-benzyloxy-6,6-bis-ethylsulfanyl-hexan-3-ol (851178-77-3) → C41H50O5S2 (851178-78-4)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 25 ℃; for 12h;

DOI:10.1016/j.tet.2005.01.119

Reference yield:

C41H50O5S2 (851178-78-4) → (2R,3S,4R,5R)-2-Allyloxy-3,4,5,6-tetrakis-benzyloxy-hexanal (851178-62-6)

Guidance literature:

With calcium carbonate; mercury dichloride; In water; acetonitrile; at 25 ℃; for 6h;

DOI:10.1016/j.tet.2005.01.119

Reference yield:

C41H50O5S2 (851178-78-4) → (2S,3R,4R,5R)-2-Allyloxy-3,4,5,6-tetrakis-benzyloxy-hexanal oxime (851178-68-2)

Guidance literature:

Multi-step reaction with 2 steps

1: HgCl₂; CaCO₃ / acetonitrile; H₂O / 6 h / 25 °C

2: NH₂OH*HCl; pyridine / methanol / 8 h / Heating

With pyridine; hydroxylamine hydrochloride; calcium carbonate; mercury dichloride; In methanol; water; acetonitrile;

DOI:10.1016/j.tet.2005.01.119

upstream raw materials:

benzyl bromide

(2R,3R,4S,5R)-5-Allyloxy-1,2,4-tris-benzyloxy-6,6-bis-ethylsulfanyl-hexan-3-ol

Downstream raw materials:

(2R,3S,4R,5R)-2-Allyloxy-3,4,5,6-tetrakis-benzyloxy-hexanal

(2S,3R,4R,5R)-2-Allyloxy-3,4,5,6-tetrakis-benzyloxy-hexanal oxime