ethyl (4R,5S)-5-(benzyloxy)-4-[1-(tert-butyl)-1,1-dimethylsilyl]oxyhexanoate

Base Information

Chemical Name:ethyl (4R,5S)-5-(benzyloxy)-4-[1-(tert-butyl)-1,1-dimethylsilyl]oxyhexanoate
CAS No.:959774-96-0
Molecular Formula:C₂₁H₃₆O₄Si
Molecular Weight:380.6
Hs Code.:

Synonyms:ethyl (4R,5S)-5-(benzyloxy)-4-[1-(tert-butyl)-1,1-dimethylsilyl]oxyhexanoate

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Chemical Property of ethyl (4R,5S)-5-(benzyloxy)-4-[1-(tert-butyl)-1,1-dimethylsilyl]oxyhexanoate

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Technology Process of ethyl (4R,5S)-5-(benzyloxy)-4-[1-(tert-butyl)-1,1-dimethylsilyl]oxyhexanoate

There total 1 articles about ethyl (4R,5S)-5-(benzyloxy)-4-[1-(tert-butyl)-1,1-dimethylsilyl]oxyhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: ethyl (4R,5S)-5-(benzyloxy)-4-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-hexenoate

: 959774-96-0
ethyl (4R,5S)-5-(benzyloxy)-4-[1-(tert-butyl)-1,1-dimethylsilyl]oxyhexanoate

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethyl acetate; at 20 ℃; for 3h;
DOI:10.1016/j.tetasy.2007.08.017

Reference yield: 82.0%

: 959774-96-0
ethyl (4R,5S)-5-(benzyloxy)-4-[1-(tert-butyl)-1,1-dimethylsilyl]oxyhexanoate

: 959774-89-1
(4R,5S)-5-(benzyloxy)-4-[1-(tert-butyl)-1,1-dimethylsilyl]oxyhexanoic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃; for 4h;
DOI:10.1016/j.tetasy.2007.08.017

Reference yield:

: 959774-96-0
ethyl (4R,5S)-5-(benzyloxy)-4-[1-(tert-butyl)-1,1-dimethylsilyl]oxyhexanoate

: C₂₆H₃₃O₅Cl₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / LiOH / H₂O; tetrahydrofuran; methanol / 4 h / 20 °C

2: triethylamine / tetrahydrofuran / 2 h / 20 °C

With lithium hydroxide; triethylamine; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.tetasy.2007.08.017