2,5-Bis-methoxymethoxy-1-methyl-3-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

Base Information

Chemical Name:2,5-Bis-methoxymethoxy-1-methyl-3-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene
CAS No.:449775-69-3
Molecular Formula:C₂₆H₄₀O₄
Molecular Weight:416.601
Hs Code.:

Synonyms:2,5-Bis-methoxymethoxy-1-methyl-3-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

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Chemical Property of 2,5-Bis-methoxymethoxy-1-methyl-3-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

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Technology Process of 2,5-Bis-methoxymethoxy-1-methyl-3-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

There total 1 articles about 2,5-Bis-methoxymethoxy-1-methyl-3-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24163-93-7,24163-94-8,56881-57-3,6874-67-5,28290-41-7
farnesyl bromide

: 50848-61-8
1-bromo-2,5-bis(methoxymethoxy)-3-methylbenzene

: 449775-69-3
2,5-Bis-methoxymethoxy-1-methyl-3-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

Guidance literature:: 1-bromo-2,5-bis(methoxymethoxy)-3-methylbenzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

farnesyl bromide; With copper(l) iodide; In tetrahydrofuran; at -78 - 20 ℃; for 1.5h;
DOI:10.1016/S0968-0896(01)00428-X

Reference yield:

: 449775-69-3
2,5-Bis-methoxymethoxy-1-methyl-3-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

: 449775-75-1
2,5-bis-methoxymethoxy-1-methyl-3-(3,7,11-trimethyl-dodecyl)-benzene

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethyl acetate; at 20 ℃; for 2h;
DOI:10.1016/S0968-0896(01)00428-X

Reference yield:

: 449775-69-3
2,5-Bis-methoxymethoxy-1-methyl-3-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

: 449775-79-5
2-Methyl-6-(3,7,11-trimethyl-dodecyl)-benzene-1,4-diol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / PtO₂ / ethyl acetate / 2 h / 20 °C

2: conc. HCl / CHCl₃; methanol / 1 h / Heating

With hydrogenchloride; hydrogen; platinum(IV) oxide; In methanol; chloroform; ethyl acetate;
DOI:10.1016/S0968-0896(01)00428-X