2-{3-[acetyl-(3-bromo-pyridin-2-yl)-amino]-propenyl}-4-(tert-butyl-dimethyl-silanyloxy)-pyrrolidine-1-carboxylic acid benzyl ester

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Chemical Name:2-{3-[acetyl-(3-bromo-pyridin-2-yl)-amino]-propenyl}-4-(tert-butyl-dimethyl-silanyloxy)-pyrrolidine-1-carboxylic acid benzyl ester
CAS No.:1003961-43-0
Molecular Formula:C₂₈H₃₈BrN₃O₄Si
Molecular Weight:588.617
Hs Code.:

Synonyms:2-{3-[acetyl-(3-bromo-pyridin-2-yl)-amino]-propenyl}-4-(tert-butyl-dimethyl-silanyloxy)-pyrrolidine-1-carboxylic acid benzyl ester

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Chemical Property of 2-{3-[acetyl-(3-bromo-pyridin-2-yl)-amino]-propenyl}-4-(tert-butyl-dimethyl-silanyloxy)-pyrrolidine-1-carboxylic acid benzyl ester

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Technology Process of 2-{3-[acetyl-(3-bromo-pyridin-2-yl)-amino]-propenyl}-4-(tert-butyl-dimethyl-silanyloxy)-pyrrolidine-1-carboxylic acid benzyl ester

There total 1 articles about 2-{3-[acetyl-(3-bromo-pyridin-2-yl)-amino]-propenyl}-4-(tert-butyl-dimethyl-silanyloxy)-pyrrolidine-1-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1174653-56-5
C₂₂H₃₅NO₆SSi

: 155444-28-3
N-(3-bromo-2-pyridinyl)acetamide

: 1003961-43-0
2-{3-[acetyl-(3-bromo-pyridin-2-yl)-amino]-propenyl}-4-(tert-butyl-dimethyl-silanyloxy)-pyrrolidine-1-carboxylic acid benzyl ester

Guidance literature:: N-(3-bromo-2-pyridinyl)acetamide; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1.25h;

C₂₂H₃₅NO₆SSi; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;

Reference yield: 59.0%

: 1003961-43-0
2-{3-[acetyl-(3-bromo-pyridin-2-yl)-amino]-propenyl}-4-(tert-butyl-dimethyl-silanyloxy)-pyrrolidine-1-carboxylic acid benzyl ester

: 1003961-44-1
C₂₈H₃₇N₃O₄Si

Guidance literature:: With tetrabutyl-ammonium chloride; sodium formate; potassium carbonate; palladium diacetate; In N,N-dimethyl-formamide; for 4h; Heating;