3,3'-bis(4'-bromophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-bis-indole

Base Information

Chemical Name:3,3'-bis(4'-bromophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-bis-indole
CAS No.:1159837-07-6
Molecular Formula:C₃₂H₂₆Br₂N₂O₄
Molecular Weight:662.377
Hs Code.:

Synonyms:3,3'-bis(4'-bromophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-bis-indole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3'-bis(4'-bromophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-bis-indole

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Technology Process of 3,3'-bis(4'-bromophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-bis-indole

There total 2 articles about 3,3'-bis(4'-bromophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-bis-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 74794-91-5
3-(4-bromophenyl)-4,6-dimethoxy-1H-indole

: 1048987-98-9
2,2'-bi[3-(4-bromophenyl)-4,6-dimethoxy]indole

: 1159837-07-6
3,3'-bis(4'-bromophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-bis-indole

Guidance literature:: 3-(4-bromophenyl)-4,6-dimethoxy-1H-indole; With sodium hydride; In dichloromethane; mineral oil; for 0.0833333h;

With trifluoromethylsulfonic anhydride; In dichloromethane; mineral oil; at 25 ℃; for 48h; Concentration; Time; Reagent/catalyst; Reactivity;
DOI:10.1016/j.tetlet.2009.03.052

Reference yield: 50.0%

: 74794-91-5
3-(4-bromophenyl)-4,6-dimethoxy-1H-indole

: 1159837-07-6
3,3'-bis(4'-bromophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-bis-indole

Guidance literature:: With tin(IV) chloride; In nitromethane; dichloromethane; acetonitrile; for 12h; Reflux;
DOI:10.1016/j.tetlet.2012.04.082

Reference yield: 80.0%

: 1159837-07-6
3,3'-bis(4'-bromophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-bis-indole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1453486-15-1
C₃₄H₂₆Br₂N₂O₆

Guidance literature:: 3,3'-bis(4'-bromophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-bis-indole; N,N-dimethyl-formamide; With trichlorophosphate; at 20 - 60 ℃; for 8.5h;

With water; sodium hydroxide; at 20 ℃; for 1h;
DOI:10.1055/s-0033-1338868