6,6-di-tert-butyl-2-(tert-butyl-dimethyl-silanyloxymethyl)-hexahydro-5,7-dioxa-2a-aza-6-sila-cyclopenta[cd]inden-1-ol

Base Information

• Chemical Name: 6,6-di-tert-butyl-2-(tert-butyl-dimethyl-silanyloxymethyl)-hexahydro-5,7-dioxa-2a-aza-6-sila-cyclopenta[cd]inden-1-ol
• CAS No.: 225113-29-1
• Molecular Formula: C₂₂H₄₅NO₄Si₂
• Molecular Weight: 443.775

Synonyms:6,6-di-tert-butyl-2-(tert-butyl-dimethyl-silanyloxymethyl)-hexahydro-5,7-dioxa-2a-aza-6-sila-cyclopenta[cd]inden-1-ol

Chemical Property of 6,6-di-tert-butyl-2-(tert-butyl-dimethyl-silanyloxymethyl)-hexahydro-5,7-dioxa-2a-aza-6-sila-cyclopenta[cd]inden-1-ol

Chemical Property:

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Technology Process of 6,6-di-tert-butyl-2-(tert-butyl-dimethyl-silanyloxymethyl)-hexahydro-5,7-dioxa-2a-aza-6-sila-cyclopenta[cd]inden-1-ol

There total 2 articles about 6,6-di-tert-butyl-2-(tert-butyl-dimethyl-silanyloxymethyl)-hexahydro-5,7-dioxa-2a-aza-6-sila-cyclopenta[cd]inden-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

Methanesulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-1-[(2S,2aR,5aS,7R,8bR)-4,4-di-tert-butyl-7-((1S,2R)-2-phenyl-cyclohexyloxy)-hexahydro-1,3,5,8-tetraoxa-8a-aza-4-sila-acenaphthylen-2-yl]-ethyl ester (225113-27-9) → (1S,2R)-trans-2-phenyl-1-cyclohexanol (34281-92-0) + 6,6-di-tert-butyl-2-(tert-butyl-dimethyl-silanyloxymethyl)-hexahydro-5,7-dioxa-2a-aza-6-sila-cyclopenta[cd]inden-1-ol (225113-29-1) + Methanesulfonic acid (1S,2S)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-((3aS,7R,7aR)-5,5-di-tert-butyl-hexahydro-4,6-dioxa-1-aza-5-sila-inden-7-yl)-2-hydroxy-ethyl ester (225113-28-0)

Guidance literature:

With hydrogen; nickel; In methanol; for 36h; under 13445.8 Torr;

DOI:10.1021/ja9829970

Reference yield: 40.0%

Methanesulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-1-[(2S,2aR,5aS,7R,8bR)-4,4-di-tert-butyl-7-((1S,2R)-2-phenyl-cyclohexyloxy)-hexahydro-1,3,5,8-tetraoxa-8a-aza-4-sila-acenaphthylen-2-yl]-ethyl ester (225113-27-9) → (1S,2R)-trans-2-phenyl-1-cyclohexanol (34281-92-0) + 6,6-di-tert-butyl-2-(tert-butyl-dimethyl-silanyloxymethyl)-hexahydro-5,7-dioxa-2a-aza-6-sila-cyclopenta[cd]inden-1-ol (225113-29-1)

Guidance literature:

With hydrogen; nickel; In methanol; for 48h; under 4137.18 Torr;

DOI:10.1021/ja9829970

upstream raw materials:

Methanesulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-1-[(2S,2aR,5aS,7R,8bR)-4,4-di-tert-butyl-7-((1S,2R)-2-phenyl-cyclohexyloxy)-hexahydro-1,3,5,8-tetraoxa-8a-aza-4-sila-acenaphthylen-2-yl]-ethyl ester

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