4-(4-bromophenyl)-5-phenyl-4H-1,2,4-triazol-3-yl hydrosulfide

Base Information

Chemical Name:4-(4-bromophenyl)-5-phenyl-4H-1,2,4-triazol-3-yl hydrosulfide
CAS No.:162221-97-8
Molecular Formula:C₁₄H₁₀BrN₃S
Molecular Weight:332.223
Hs Code.:
Mol file:162221-97-8.mol

Synonyms:4-(4-bromophenyl)-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4-bromophenyl)-5-phenyl-4H-1,2,4-triazol-3-yl hydrosulfide

Chemical Property:

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Technology Process of 4-(4-bromophenyl)-5-phenyl-4H-1,2,4-triazol-3-yl hydrosulfide

There total 7 articles about 4-(4-bromophenyl)-5-phenyl-4H-1,2,4-triazol-3-yl hydrosulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 38240-75-4
1-benzoyl-4-(4-bromophenyl)thiosemicarbazide

: 162221-97-8
4-(4-bromophenyl)-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione

Guidance literature:: With sodium hydroxide; for 2h; Reflux;
DOI:10.1007/s00044-012-0248-y

Reference yield: 74.0%

: C₁₄H₁₂BrN₃S

: 162221-97-8
4-(4-bromophenyl)-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione

Guidance literature:: With copper(ll) bromide; In dimethyl sulfoxide; at 80 ℃; for 1h;
DOI:10.1021/acs.joc.5b00956

Reference yield:

: 613-94-5
benzoic acid hydrazide

: 162221-97-8
4-(4-bromophenyl)-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 0.5 h / Heating

2: aq. NaOH / 2 h / Heating

With sodium hydroxide; In ethanol;
DOI:10.1080/104265090517280