dodecacarbonyldihydridotriosmium

Base Information

Chemical Name:dodecacarbonyldihydridotriosmium
CAS No.:12560-48-4
Molecular Formula:C₁₂H₂O₁₂Os₃
Molecular Weight:908.741
Hs Code.:

Synonyms:dodecacarbonyldihydridotriosmium

Suppliers and Price of dodecacarbonyldihydridotriosmium

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dodecacarbonyldihydridotriosmium

Chemical Property:

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Technology Process of dodecacarbonyldihydridotriosmium

There total 1 articles about dodecacarbonyldihydridotriosmium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25685-05-6
octacarbonyldihydridodiosmium

: 15696-40-9
dodecacarbonyl triosmium

: 22372-70-9,18972-42-4
H₂Os(CO)4

: 12560-48-4
dodecacarbonyldihydridotriosmium

: 41766-80-7
Os3(μ-H)2(CO)10

: 60645-65-0
Os₄(CO)16H₂

Guidance literature:: In neat (no solvent); sealed tube (vac.), 135°C, 20 min; cooling, removal of volatiles (reduced pressure); product mixt. not sepd., detd. by IR spectroscopy;
DOI:10.1039/DT9770000089

Reference yield: 70.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 12560-48-4
dodecacarbonyldihydridotriosmium

: Os₃(CO)12(AuP(C₆H₅)3)2

Guidance literature:: With diethylamine; In not given; N2-atmosphere; recrystn.;

Reference yield: 57.0%

: 12560-48-4
dodecacarbonyldihydridotriosmium

: 639-58-7
triphenyltin chloride

: Os₃(CO)12(Sn(C₆H₅)3)2

Guidance literature:: With diethylamine; In dichloromethane; N2-atmosphere; 2 equiv. Ph3SnCl, excess Et2NH, stirring for 45 min; solvent removal (reduced pressure), recrystn. (CH2Cl2/MeOH);