3-{2-[3-tert-butoxycarbonyl-2-(2-tritylsulfanyl-acetylamino)-propionyl amino]-2-carboxy-ethyl}-indole-1-carboxylic acid tert-butyl ester

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Chemical Name:3-{2-[3-tert-butoxycarbonyl-2-(2-tritylsulfanyl-acetylamino)-propionyl amino]-2-carboxy-ethyl}-indole-1-carboxylic acid tert-butyl ester
CAS No.:708269-66-3
Molecular Formula:C₄₅H₄₉N₃O₈S
Molecular Weight:791.965
Hs Code.:

Synonyms:3-{2-[3-tert-butoxycarbonyl-2-(2-tritylsulfanyl-acetylamino)-propionyl amino]-2-carboxy-ethyl}-indole-1-carboxylic acid tert-butyl ester

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Chemical Property of 3-{2-[3-tert-butoxycarbonyl-2-(2-tritylsulfanyl-acetylamino)-propionyl amino]-2-carboxy-ethyl}-indole-1-carboxylic acid tert-butyl ester

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Technology Process of 3-{2-[3-tert-butoxycarbonyl-2-(2-tritylsulfanyl-acetylamino)-propionyl amino]-2-carboxy-ethyl}-indole-1-carboxylic acid tert-butyl ester

There total 1 articles about 3-{2-[3-tert-butoxycarbonyl-2-(2-tritylsulfanyl-acetylamino)-propionyl amino]-2-carboxy-ethyl}-indole-1-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: H-Trp (BOC)-2-CI-Trt

: 34914-36-8
2-(triphenylmethylthio)ethanoic acid

: 129460-09-9,134098-70-7
Fmoc-Asp-O-t-Bu

: 708269-66-3
3-{2-[3-tert-butoxycarbonyl-2-(2-tritylsulfanyl-acetylamino)-propionyl amino]-2-carboxy-ethyl}-indole-1-carboxylic acid tert-butyl ester

Guidance literature:: Fmoc-Asp-O-t-Bu; With benzotriazol-1-ol; diisopropyl-carbodiimide; In 1-methyl-pyrrolidin-2-one; at 0 - 20 ℃; for 0.5h;

H-Trp (BOC)-2-CI-Trt; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 2h;

2-(triphenylmethylthio)ethanoic acid; With piperidine; more than 3 stages;