dicarbonyldichlorobis(triphenylphosphine)bis(μ-4-chloropyrazolyl)diiridium(II)

Base Information

Chemical Name:dicarbonyldichlorobis(triphenylphosphine)bis(μ-4-chloropyrazolyl)diiridium(II)
CAS No.:80461-90-1
Molecular Formula:C₄₄H₃₄Cl₄Ir₂N₄O₂P₂
Molecular Weight:1408.84
Hs Code.:

Synonyms:dicarbonyldichlorobis(triphenylphosphine)bis(μ-4-chloropyrazolyl)diiridium(II)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dicarbonyldichlorobis(triphenylphosphine)bis(μ-4-chloropyrazolyl)diiridium(II)

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Technology Process of dicarbonyldichlorobis(triphenylphosphine)bis(μ-4-chloropyrazolyl)diiridium(II)

There total 4 articles about dicarbonyldichlorobis(triphenylphosphine)bis(μ-4-chloropyrazolyl)diiridium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 98420-38-3
dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

: 80461-90-1
dicarbonyldichlorobis(triphenylphosphine)bis(μ-4-chloropyrazolyl)diiridium(II)

Guidance literature:: With Cl₂; In tetrahydrofuran; under N2, dry Cl2 was bubbled into soln. of Ir-complex in THF; concd., stood at 0°C for 24 h, recrystd. from CH2Cl2; elem. anal.;

Reference yield:

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 80461-90-1
[Ir(CO)(triphenlyphosphine)(Cl)(μ-4-Cl-pyrazolyl)]2*2CH2Cl2

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: Cl₂

With Cl₂; In tetrahydrofuran;
DOI:10.1021/ja00367a075