2-(4-amino-2-butoxy-6-methylpyridin-3-yl)-4-bromo-N,N-diisopropylbenzamide

Base Information

Chemical Name:2-(4-amino-2-butoxy-6-methylpyridin-3-yl)-4-bromo-N,N-diisopropylbenzamide
CAS No.:1058129-60-4
Molecular Formula:C₂₃H₃₂BrN₃O₂
Molecular Weight:462.43
Hs Code.:

Synonyms:2-(4-amino-2-butoxy-6-methylpyridin-3-yl)-4-bromo-N,N-diisopropylbenzamide

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Chemical Property of 2-(4-amino-2-butoxy-6-methylpyridin-3-yl)-4-bromo-N,N-diisopropylbenzamide

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Technology Process of 2-(4-amino-2-butoxy-6-methylpyridin-3-yl)-4-bromo-N,N-diisopropylbenzamide

There total 9 articles about 2-(4-amino-2-butoxy-6-methylpyridin-3-yl)-4-bromo-N,N-diisopropylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1058129-59-1
2-butoxy-3-iodo-6-methylpyridin-4-amine

: 1058129-82-0
{5-bromo-2-[(diisopropylamino)carbonyl]phenyl}boronic acid

: 1058129-60-4
2-(4-amino-2-butoxy-6-methylpyridin-3-yl)-4-bromo-N,N-diisopropylbenzamide

Guidance literature:: With caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; for 3h; Heating / reflux;

Reference yield:

: 79055-63-3
2-chloro-6-methylpyridin-4-amine

: 1058129-60-4
2-(4-amino-2-butoxy-6-methylpyridin-3-yl)-4-bromo-N,N-diisopropylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / 10 h / Heating / reflux

2: N-iodo-succinimide / tetrahydrofuran / 0.03 h / -78 °C

3: caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 3 h / Heating / reflux

With sodium hydroxide; N-iodo-succinimide; caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 18368-63-3
6-chloro-2-picoline

: 1058129-60-4
2-(4-amino-2-butoxy-6-methylpyridin-3-yl)-4-bromo-N,N-diisopropylbenzamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 8 h / 40 °C

1.2: pH 7.5

2.1: sulfuric acid; nitric acid / 3 h / 0 - 90 °C

3.1: ammonia; iron / ethanol; water / 3 h / 90 °C

4.1: sodium hydroxide / 10 h / Heating / reflux

5.1: N-iodo-succinimide / tetrahydrofuran / 0.03 h / -78 °C

6.1: caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 3 h / Heating / reflux

With sodium hydroxide; N-iodo-succinimide; sulfuric acid; ammonia; nitric acid; iron; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water;