(2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-2-methyl-3-triethylsilyloxypropanal

Base Information

Chemical Name:(2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-2-methyl-3-triethylsilyloxypropanal
CAS No.:1192065-09-0
Molecular Formula:C₂₆H₄₄O₄Si
Molecular Weight:448.718
Hs Code.:

Synonyms:(2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-2-methyl-3-triethylsilyloxypropanal

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Chemical Property of (2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-2-methyl-3-triethylsilyloxypropanal

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Technology Process of (2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-2-methyl-3-triethylsilyloxypropanal

There total 1 articles about (2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-2-methyl-3-triethylsilyloxypropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1192065-30-7
(2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-N-methoxy-N,2-dimethyl-3-triethylsilyloxypropionamide

: 1192065-09-0
(2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-2-methyl-3-triethylsilyloxypropanal

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 ℃; for 3h; Inert atmosphere;
DOI:10.1039/b909646a

Reference yield: 99.0%

: 1192065-09-0
(2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-2-methyl-3-triethylsilyloxypropanal

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1192065-37-4
{(1R,2S)-1-[3,5-dimethoxy-4-((S)-oct-1-en-4-yl)phenyl]-2-methylbut-3-enyloxy}triethylsilane

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.25h; Inert atmosphere;

(2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-2-methyl-3-triethylsilyloxypropanal; In tetrahydrofuran; toluene; at -78 ℃; Inert atmosphere;
DOI:10.1039/b909646a

Reference yield: 94.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 1192065-09-0
(2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-2-methyl-3-triethylsilyloxypropanal

: 1192065-31-8
(4S,5R,E)-ethyl 5-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-4-methyl-5-triethylsilyloxypent-2-enoate

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.166667h; Inert atmosphere;

(2R,3R)-3-{3,5-dimethoxy-4-[(S)-oct-1-en-4-yl]phenyl}-2-methyl-3-triethylsilyloxypropanal; In tetrahydrofuran; mineral oil; at 0 ℃; Inert atmosphere;
DOI:10.1039/b909646a