2,2-dimethyl-propionic acid 2-acetyl-4-[2-(2,2-dimethyl-propionyloxy)-ethyl]-3,5-dimethyl-benzyl ester

Base Information

Chemical Name:2,2-dimethyl-propionic acid 2-acetyl-4-[2-(2,2-dimethyl-propionyloxy)-ethyl]-3,5-dimethyl-benzyl ester
CAS No.:910470-87-0
Molecular Formula:C₂₃H₃₄O₅
Molecular Weight:390.52
Hs Code.:

Synonyms:2,2-dimethyl-propionic acid 2-acetyl-4-[2-(2,2-dimethyl-propionyloxy)-ethyl]-3,5-dimethyl-benzyl ester

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Chemical Property of 2,2-dimethyl-propionic acid 2-acetyl-4-[2-(2,2-dimethyl-propionyloxy)-ethyl]-3,5-dimethyl-benzyl ester

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Technology Process of 2,2-dimethyl-propionic acid 2-acetyl-4-[2-(2,2-dimethyl-propionyloxy)-ethyl]-3,5-dimethyl-benzyl ester

There total 12 articles about 2,2-dimethyl-propionic acid 2-acetyl-4-[2-(2,2-dimethyl-propionyloxy)-ethyl]-3,5-dimethyl-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 910470-86-9
2,2-dimethyl-propionic acid 4-[2-(2,2-dimethyl-propionyloxy)-ethyl]-2-ethynyl-3,5-dimethyl-benzyl ester

: 910470-87-0
2,2-dimethyl-propionic acid 2-acetyl-4-[2-(2,2-dimethyl-propionyloxy)-ethyl]-3,5-dimethyl-benzyl ester

Guidance literature:: With trifluorormethanesulfonic acid; methyl(triphenylphosphine)gold(I); In methanol; water;
DOI:10.1055/s-2006-944190

Reference yield:

: 341006-48-2
methyl 3,5-dimethyl-4-{[(trifluoromethyl)sulfonyl]oxy}benzoate

: 910470-87-0
2,2-dimethyl-propionic acid 2-acetyl-4-[2-(2,2-dimethyl-propionyloxy)-ethyl]-3,5-dimethyl-benzyl ester

Guidance literature:: Multi-step reaction with 9 steps

1.1: 92 percent / Et₃N / Pd(PPh₃)2Cl₂

2.1: BH₃*THF / tetrahydrofuran / 2 h / 0 °C

2.2: 44 percent / NaOH; aq. H₂O₂ / tetrahydrofuran / 2 h / 0 °C

3.1: 76 percent / LiAlH₄

4.1: 96 percent / pyridine; DMAP

5.1: 91 percent / I₂; PhI(OOCCF₃)2

6.1: 90 percent / pyridine

7.1: 92 percent / Et₃N / Pd(PPh₃)2Cl₂

8.1: 66 percent / KF; 18-crown-6

9.1: 77 percent / TfOH / Au(PPh₃)CH₃ / methanol; H₂O

With pyridine; dmap; potassium fluoride; lithium aluminium tetrahydride; borane-THF; 18-crown-6 ether; trifluorormethanesulfonic acid; iodine; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; bis-triphenylphosphine-palladium(II) chloride; methyl(triphenylphosphine)gold(I); In tetrahydrofuran; methanol; water; 1.1: Sonogashira coupling / 7.1: Sonogashira coupling;
DOI:10.1055/s-2006-944190

Reference yield:

: 910470-69-8
2-(4-hydroxymethyl-2,6-dimethyl-phenyl)-ethanol

: 910470-87-0
2,2-dimethyl-propionic acid 2-acetyl-4-[2-(2,2-dimethyl-propionyloxy)-ethyl]-3,5-dimethyl-benzyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / pyridine; DMAP

2: 91 percent / I₂; PhI(OOCCF₃)2

3: 90 percent / pyridine

4: 92 percent / Et₃N / Pd(PPh₃)2Cl₂

5: 66 percent / KF; 18-crown-6

6: 77 percent / TfOH / Au(PPh₃)CH₃ / methanol; H₂O

With pyridine; dmap; potassium fluoride; 18-crown-6 ether; trifluorormethanesulfonic acid; iodine; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; bis-triphenylphosphine-palladium(II) chloride; methyl(triphenylphosphine)gold(I); In methanol; water; 4: Sonogashira coupling;
DOI:10.1055/s-2006-944190