ethyl 2-amino-2-[1-(3-fluorophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate

Base Information

• Chemical Name: ethyl 2-amino-2-[1-(3-fluorophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate
• CAS No.: 1363375-47-6
• Molecular Formula: C₂₂H₂₃FN₂O₄S
• Molecular Weight: 430.5

Synonyms:ethyl 2-amino-2-[1-(3-fluorophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate

Chemical Property of ethyl 2-amino-2-[1-(3-fluorophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate

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Technology Process of ethyl 2-amino-2-[1-(3-fluorophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate

There total 7 articles about ethyl 2-amino-2-[1-(3-fluorophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

ethyl 2-[1-(3-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl]-2-(hydroxylamino)ylidene-acetate → ethyl 2-amino-2-[1-(3-fluorophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate (1363375-47-6)

Guidance literature:

With formic acid; zinc; In ethanol; at 0 - 20 ℃; for 20h;

DOI:10.1016/j.bmc.2013.12.008

Reference yield: 47.0%

ethyl 2-(hydroxyimino)-2-[2-methyl-5-[4-(methylsulfonyl)phenyl]-1-(3-fluorophenyl)-1H-pyrrol-3-yl]acetate → ethyl 2-amino-2-[1-(3-fluorophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate (1363375-47-6)

Guidance literature:

With formic acid; zinc; In ethanol; at 0 - 20 ℃;

DOI:10.1016/j.ejmech.2012.10.014

Reference yield: 47.0%

→ ethyl 2-amino-2-[1-(3-fluorophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate (1363375-47-6)

Guidance literature:

upstream raw materials:

1-[4-(methylthio)phenyl]pentane-1,4-dione

1-[4-(methylsulfonyl)phenyl]pentane-1,4-dione

4-(Methylthio)benzaldehyde

Downstream raw materials:

ethyl N-(benzyloxycarbonyl)-2-amino-2-[1-(3-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl]-acetate

N-(tert-butoxycarbonyl)-2-[1-(3-fluorophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]-2-amino-acetic acid

N-(benzyloxy)carbonyl-2-[1-(3-fluorophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]-2-amino-acetic acid

3-(nitrooxy)propyl N-(tert-butoxycarbonyl)-2-(1-(3-fluorophenyl)-2-methyl-5-(4-(methylsulfonyl)phenyl)-1H-pyrrol-3-yl)-2-amino-acetate

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