(3S,5R,1'S,4''R)-3-<4-(1'-<2'',2''-dimethyl-1'',3''-dioxolan-4''-yl>ethyl)phenyl>-5-(trimethylsilyl)cyclo-hexanone

Base Information

Chemical Name:(3S,5R,1'S,4''R)-3-<4-(1'-<2'',2''-dimethyl-1'',3''-dioxolan-4''-yl>ethyl)phenyl>-5-(trimethylsilyl)cyclo-hexanone
CAS No.:155907-20-3
Molecular Formula:C₂₂H₃₄O₃Si
Molecular Weight:374.596
Hs Code.:

Synonyms:(3S,5R,1'S,4''R)-3-<4-(1'-<2'',2''-dimethyl-1'',3''-dioxolan-4''-yl>ethyl)phenyl>-5-(trimethylsilyl)cyclo-hexanone

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Chemical Property of (3S,5R,1'S,4''R)-3-<4-(1'-<2'',2''-dimethyl-1'',3''-dioxolan-4''-yl>ethyl)phenyl>-5-(trimethylsilyl)cyclo-hexanone

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Technology Process of (3S,5R,1'S,4''R)-3-<4-(1'-<2'',2''-dimethyl-1'',3''-dioxolan-4''-yl>ethyl)phenyl>-5-(trimethylsilyl)cyclo-hexanone

There total 5 articles about (3S,5R,1'S,4''R)-3-<4-(1'-<2'',2''-dimethyl-1'',3''-dioxolan-4''-yl>ethyl)phenyl>-5-(trimethylsilyl)cyclo-hexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116215-94-2
(R)-(-)-5-trimethylsilyl-2-cyclohexenone

: 155907-20-3
(3S,5R,1'S,4''R)-3-<4-(1'-<2'',2''-dimethyl-1'',3''-dioxolan-4''-yl>ethyl)phenyl>-5-(trimethylsilyl)cyclo-hexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg, 2.) CuBr*SMe₂ / 2.) HMPA

2: KF / methanol

With potassium fluoride; copper(I) bromide dimethylsulfide complex; magnesium; In methanol;
DOI:10.1016/S0040-4039(00)79970-9

Reference yield:

: 151774-96-8
(4R,1'S)-4-<1'-(4''-bromophenyl)ethyl>-2,2-dimethyl-1,3-dioxolane

: 155907-20-3
(3S,5R,1'S,4''R)-3-<4-(1'-<2'',2''-dimethyl-1'',3''-dioxolan-4''-yl>ethyl)phenyl>-5-(trimethylsilyl)cyclo-hexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg, 2.) CuBr*SMe₂ / 2.) HMPA

2: KF / methanol

With potassium fluoride; copper(I) bromide dimethylsulfide complex; magnesium; In methanol;
DOI:10.1016/S0040-4039(00)79970-9

Reference yield:

: C₁₀H₁₃BrO₂

: 155907-20-3
(3S,5R,1'S,4''R)-3-<4-(1'-<2'',2''-dimethyl-1'',3''-dioxolan-4''-yl>ethyl)phenyl>-5-(trimethylsilyl)cyclo-hexanone

Guidance literature:: Multi-step reaction with 3 steps

2: 1.) Mg, 2.) CuBr*SMe₂ / 2.) HMPA

3: KF / methanol

With potassium fluoride; copper(I) bromide dimethylsulfide complex; magnesium; In methanol;
DOI:10.1016/S0040-4039(00)79970-9