(R)-2,2-Dimethyl-4-{(S)-1-[4-((1R,5R)-5-trimethylsilanyl-3-trimethylsilanyloxy-cyclohex-2-enyl)-phenyl]-ethyl}-[1,3]dioxolane

Base Information

Chemical Name:(R)-2,2-Dimethyl-4-{(S)-1-[4-((1R,5R)-5-trimethylsilanyl-3-trimethylsilanyloxy-cyclohex-2-enyl)-phenyl]-ethyl}-[1,3]dioxolane
CAS No.:155907-19-0
Molecular Formula:C₂₅H₄₂O₃Si₂
Molecular Weight:446.778
Hs Code.:

Synonyms:(R)-2,2-Dimethyl-4-{(S)-1-[4-((1R,5R)-5-trimethylsilanyl-3-trimethylsilanyloxy-cyclohex-2-enyl)-phenyl]-ethyl}-[1,3]dioxolane

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Chemical Property of (R)-2,2-Dimethyl-4-{(S)-1-[4-((1R,5R)-5-trimethylsilanyl-3-trimethylsilanyloxy-cyclohex-2-enyl)-phenyl]-ethyl}-[1,3]dioxolane

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Technology Process of (R)-2,2-Dimethyl-4-{(S)-1-[4-((1R,5R)-5-trimethylsilanyl-3-trimethylsilanyloxy-cyclohex-2-enyl)-phenyl]-ethyl}-[1,3]dioxolane

There total 2 articles about (R)-2,2-Dimethyl-4-{(S)-1-[4-((1R,5R)-5-trimethylsilanyl-3-trimethylsilanyloxy-cyclohex-2-enyl)-phenyl]-ethyl}-[1,3]dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₃BrO₂

: 155907-19-0
(R)-2,2-Dimethyl-4-{(S)-1-[4-((1R,5R)-5-trimethylsilanyl-3-trimethylsilanyloxy-cyclohex-2-enyl)-phenyl]-ethyl}-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) Mg, 2.) CuBr*SMe₂ / 2.) HMPA

With copper(I) bromide dimethylsulfide complex; magnesium;
DOI:10.1016/S0040-4039(00)79970-9

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 116215-94-2
(R)-(-)-5-trimethylsilyl-2-cyclohexenone

: 151774-96-8
(4R,1'S)-4-<1'-(4''-bromophenyl)ethyl>-2,2-dimethyl-1,3-dioxolane

: 155907-19-0
(R)-2,2-Dimethyl-4-{(S)-1-[4-((1R,5R)-5-trimethylsilanyl-3-trimethylsilanyloxy-cyclohex-2-enyl)-phenyl]-ethyl}-[1,3]dioxolane

Guidance literature:: With copper(I) bromide dimethylsulfide complex; magnesium; Multistep reaction; 2.) HMPA;
DOI:10.1016/S0040-4039(00)79970-9

Reference yield:

: 155907-19-0
(R)-2,2-Dimethyl-4-{(S)-1-[4-((1R,5R)-5-trimethylsilanyl-3-trimethylsilanyloxy-cyclohex-2-enyl)-phenyl]-ethyl}-[1,3]dioxolane

: (S)-2-(4-{(R)-3-[(E)-Hydroxyimino]-cyclohexyl}-phenyl)-propionic acid

Guidance literature:: Multi-step reaction with 5 steps

1: KF / methanol

2: CuCl₂

3: 62 percent / H₂ / Pd/C

4: 82 percent / NaIO₄ / RuCl₃

5: HONH₂*HCl / pyridine

With potassium fluoride; sodium periodate; hydroxylamine hydrochloride; hydrogen; copper dichloride; ruthenium trichloride; palladium on activated charcoal; In pyridine; methanol;
DOI:10.1016/S0040-4039(00)79970-9