N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

Base Information

Chemical Name:N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<amino>-2,4,6-triiodo-1,3-benzenedicarboxamide
CAS No.:148051-10-9
Molecular Formula:C₂₇H₃₁I₄N₃O₁₁
Molecular Weight:1081.17
Hs Code.:

N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<<dihydro-5-(iodomethyl)-2(3H)-furanylidene>amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

Synonyms:N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

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Chemical Property of N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

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Technology Process of N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

There total 4 articles about N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<amino>-2,4,6-triiodo-1,3-benzenedicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.5%

: 148051-09-6
N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-2,4,6-triiodo-5-<(1-oxo-4-pentenoyl)amino>-1,3-benzenedicarboxamide

: 148051-10-9
N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

Guidance literature:: With N-iodo-succinimide; In chloroform; at 50 ℃; for 1h;
DOI:10.1021/jo00119a020

Reference yield:

: 39716-58-0
pent-4-enoyl chloride

: 148051-10-9
N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / N,N-dimethyl-acetamide / 1.) 5 deg C, 0.5 h, 2.) room temp., 20 h

2: NaOMe / methanol / 4 h

3: 1.) N-iodosuccinimide, 2.) pyridine / 1.) water, MeOH, room temp.

With pyridine; N-iodo-succinimide; sodium methylate; In methanol; N,N-dimethyl acetamide;
DOI:10.1021/jo00119a020

Reference yield:

: 148051-08-5
N,N'-bis[2-(acetyloxy)-1-[(acetyloxy)methyl]ethyl]-5-amino-2,4,6-triiodo-1,3-benzenedicarboxamide

: 148051-10-9
N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / N,N-dimethyl-acetamide / 1.) 5 deg C, 0.5 h, 2.) room temp., 20 h

2: NaOMe / methanol / 4 h

3: 1.) N-iodosuccinimide, 2.) pyridine / 1.) water, MeOH, room temp.

With pyridine; N-iodo-succinimide; sodium methylate; In methanol; N,N-dimethyl acetamide;
DOI:10.1021/jo00119a020