1-O-acetyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6-di-O-benzyl-7-hydroxyxanthone

Base Information

Chemical Name:1-O-acetyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6-di-O-benzyl-7-hydroxyxanthone
CAS No.:1609192-23-5
Molecular Formula:C₄₃H₄₀O₁₆
Molecular Weight:812.781
Hs Code.:

Synonyms:1-O-acetyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6-di-O-benzyl-7-hydroxyxanthone

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Chemical Property of 1-O-acetyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6-di-O-benzyl-7-hydroxyxanthone

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Technology Process of 1-O-acetyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6-di-O-benzyl-7-hydroxyxanthone

There total 7 articles about 1-O-acetyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6-di-O-benzyl-7-hydroxyxanthone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 31002-09-2
1,7-Di-O-acetyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6-di-O-benzylxanthone

: 1609192-23-5
1-O-acetyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6-di-O-benzyl-7-hydroxyxanthone

: 1609192-24-6
1,7-dihydroxy-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6-di-O-benzylxanthone

Guidance literature:: With ammonium acetate; In methanol; water; acetone; at 20 - 60 ℃;
DOI:10.1016/j.tetlet.2014.03.129

Reference yield: 20.0%

: 1-O-acetyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6,7-trihydroxyxanthone

: 100-39-0
benzyl bromide

: 1609192-23-5
1-O-acetyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6-di-O-benzyl-7-hydroxyxanthone

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; regioselective reaction;
DOI:10.1016/j.tetlet.2014.03.129

Reference yield:

: Mangiferin

: 1609192-23-5
1-O-acetyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,6-di-O-benzyl-7-hydroxyxanthone

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 12 h / 20 °C

2: ammonium acetate / methanol; water / 3 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 60 °C

With pyridine; ammonium acetate; potassium carbonate; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2014.03.129