6-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-hexanoic acid benzyl-carbamoylmethyl-amide

Base Information

Chemical Name:6-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-hexanoic acid benzyl-carbamoylmethyl-amide
CAS No.:345945-45-1
Molecular Formula:C₂₃H₂₅N₃O₄
Molecular Weight:407.469
Hs Code.:

Synonyms:6-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-hexanoic acid benzyl-carbamoylmethyl-amide

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Chemical Property of 6-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-hexanoic acid benzyl-carbamoylmethyl-amide

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Technology Process of 6-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-hexanoic acid benzyl-carbamoylmethyl-amide

There total 5 articles about 6-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-hexanoic acid benzyl-carbamoylmethyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31968-60-2
6-phthalimidohexanoyl chloride

: 39796-49-1
benzylaminodiacetamide

: 345945-45-1
6-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-hexanoic acid benzyl-carbamoylmethyl-amide

Guidance literature:: With triethylamine; In chloroform; for 2h; Yield given; Ambient temperature;
DOI:10.1055/s-1983-30329

Reference yield:

: 85-44-9
phthalic anhydride

: 345945-45-1
6-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-hexanoic acid benzyl-carbamoylmethyl-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 0.5 h / 145 - 150 °C

2: SOCl₂ / 1 h / Heating

3: triethylamine / CHCl₃ / 2 h / Ambient temperature

With thionyl chloride; triethylamine; In chloroform;
DOI:10.1055/s-1983-30329

Reference yield:

: 4443-26-9
6-phthalimidohexanoic acid

: 345945-45-1
6-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-hexanoic acid benzyl-carbamoylmethyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 1 h / Heating

2: triethylamine / CHCl₃ / 2 h / Ambient temperature

With thionyl chloride; triethylamine; In chloroform;
DOI:10.1055/s-1983-30329