3-(ethoxycarbonylacetyl)-1,3-bis[4-nitro-2-(trifluoromethyl)phenyl]triazene

Base Information

Chemical Name:3-(ethoxycarbonylacetyl)-1,3-bis[4-nitro-2-(trifluoromethyl)phenyl]triazene
CAS No.:1313389-49-9
Molecular Formula:C₁₉H₁₃F₆N₅O₇
Molecular Weight:537.332
Hs Code.:

Synonyms:3-(ethoxycarbonylacetyl)-1,3-bis[4-nitro-2-(trifluoromethyl)phenyl]triazene

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Chemical Property of 3-(ethoxycarbonylacetyl)-1,3-bis[4-nitro-2-(trifluoromethyl)phenyl]triazene

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Technology Process of 3-(ethoxycarbonylacetyl)-1,3-bis[4-nitro-2-(trifluoromethyl)phenyl]triazene

There total 2 articles about 3-(ethoxycarbonylacetyl)-1,3-bis[4-nitro-2-(trifluoromethyl)phenyl]triazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1243357-92-7
1,3-bis[4-nitro-2-(trifluoromethyl)phenyl]triazene

: 36239-09-5
ethyl chlorocarbonylacetate

: 1313389-49-9
3-(ethoxycarbonylacetyl)-1,3-bis[4-nitro-2-(trifluoromethyl)phenyl]triazene

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 0.75h;
DOI:10.1016/j.ejmech.2011.04.024

Reference yield:

: 121-01-7
4-nitro-2-trifluoromethyl-aniline

: 1313389-49-9
3-(ethoxycarbonylacetyl)-1,3-bis[4-nitro-2-(trifluoromethyl)phenyl]triazene

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; sodium nitrite / water / 48 h / 0 - 20 °C

2: triethylamine / acetonitrile / 0.75 h / 20 °C

With hydrogenchloride; triethylamine; sodium nitrite; In water; acetonitrile;
DOI:10.1016/j.ejmech.2011.04.024