(R_s, S_c)-4-phenyl-N-(2-chlorotetrafluoroethanesulfinyl)oxazolidin-2-one

Base Information

• Chemical Name: (R_s, S_c)-4-phenyl-N-(2-chlorotetrafluoroethanesulfinyl)oxazolidin-2-one
• CAS No.: 1262682-98-3
• Molecular Formula: C₁₁H₈ClF₄NO₃S
• Molecular Weight: 345.702

Synonyms:(R_s, S_c)-4-phenyl-N-(2-chlorotetrafluoroethanesulfinyl)oxazolidin-2-one

Chemical Property of (R_s, S_c)-4-phenyl-N-(2-chlorotetrafluoroethanesulfinyl)oxazolidin-2-one

Chemical Property:

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Technology Process of (R_s, S_c)-4-phenyl-N-(2-chlorotetrafluoroethanesulfinyl)oxazolidin-2-one

There total 2 articles about (R_s, S_c)-4-phenyl-N-(2-chlorotetrafluoroethanesulfinyl)oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-1,1,2,2-tetrafluoroethanesulfinyl chloride + (S)-4-phenyl-2-oxazolidinone (99395-88-7,7480-32-2) → (Rs, Sc)-4-phenyl-N-(2-chlorotetrafluoroethanesulfinyl)oxazolidin-2-one (1262682-98-3)

Guidance literature:

(S)-4-phenyl-2-oxazolidinone; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

2-chloro-1,1,2,2-tetrafluoroethanesulfinyl chloride; In tetrahydrofuran; hexane; at -78 ℃; for 3h; Inert atmosphere;

DOI:10.1021/jo500008e

Reference yield:

2-chloro-1,1,2,2-tetrafluoroethanesulfinyl chloride + (S)-4-phenyl-2-oxazolidinone (99395-88-7,7480-32-2) → (Rs, Sc)-4-phenyl-N-(2-chlorotetrafluoroethanesulfinyl)oxazolidin-2-one (1262682-98-3) + (S(S),4S)-4-phenyl-N-(2-chlorotetrafluoroethanesulfinyl)oxazolidin-2-one (1303994-24-2)

Guidance literature:

(S)-4-phenyl-2-oxazolidinone; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

2-chloro-1,1,2,2-tetrafluoroethanesulfinyl chloride; In tetrahydrofuran; hexane; at -78 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;

DOI:10.1021/jo200119x

upstream raw materials:

(S)-4-phenyl-2-oxazolidinone

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