N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycinsolanesylester

Base Information

Chemical Name:N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycinsolanesylester
CAS No.:103669-59-6
Molecular Formula:C₆₉H₁₀₁NO₁₃
Molecular Weight:1152.56
Hs Code.:

Synonyms:N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycinsolanesylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycinsolanesylester

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Technology Process of N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycinsolanesylester

There total 3 articles about N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycinsolanesylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 52610-77-2
solanesyl bromide

: 103669-98-3
N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycin

: 103669-59-6
N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycinsolanesylester

Guidance literature:: With N-cyclohexyl-cyclohexanamine; In tetrahydrofuran; for 15h; Heating;

Reference yield:

: 53555-69-4
2,3,4,5,6-penta-O-acetyl-D-gluconoyl chloride

: 103669-59-6
N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycinsolanesylester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / CH₂Cl₂ / 2 h / 25 °C

2: 61 percent / dicyclohexylamine / tetrahydrofuran / 15 h / Heating

With N-cyclohexyl-cyclohexanamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 75247-41-5
N-Trimethylsilyl-DL-2-phenylglycin-trimethylsilylester

: 103669-59-6
N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycinsolanesylester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / CH₂Cl₂ / 2 h / 25 °C

2: 61 percent / dicyclohexylamine / tetrahydrofuran / 15 h / Heating

With N-cyclohexyl-cyclohexanamine; In tetrahydrofuran; dichloromethane;