(+)-(1S,5R,6S)-N-(6-acetoxy-5-isopropyl-2-methyl-cyclohex-2-enyl)-N-methyl-N-(2-prop-2-ynyl)-amine

Base Information

Chemical Name:(+)-(1S,5R,6S)-N-(6-acetoxy-5-isopropyl-2-methyl-cyclohex-2-enyl)-N-methyl-N-(2-prop-2-ynyl)-amine
CAS No.:242130-28-5
Molecular Formula:C₁₆H₂₅NO₂
Molecular Weight:263.38
Hs Code.:

Synonyms:(+)-(1S,5R,6S)-N-(6-acetoxy-5-isopropyl-2-methyl-cyclohex-2-enyl)-N-methyl-N-(2-prop-2-ynyl)-amine

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Chemical Property of (+)-(1S,5R,6S)-N-(6-acetoxy-5-isopropyl-2-methyl-cyclohex-2-enyl)-N-methyl-N-(2-prop-2-ynyl)-amine

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (+)-(1S,5R,6S)-N-(6-acetoxy-5-isopropyl-2-methyl-cyclohex-2-enyl)-N-methyl-N-(2-prop-2-ynyl)-amine

There total 7 articles about (+)-(1S,5R,6S)-N-(6-acetoxy-5-isopropyl-2-methyl-cyclohex-2-enyl)-N-methyl-N-(2-prop-2-ynyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₂H₁₉NO₃

: 242130-28-5
(+)-(1S,5R,6S)-N-(6-acetoxy-5-isopropyl-2-methyl-cyclohex-2-enyl)-N-methyl-N-(2-prop-2-ynyl)-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 24.5 g / Et₃N / tetrahydrofuran / 2 h / 20 °C

2: 71 percent / Bu₃SnH; 1,1'-azobis(cyclohexanecarbonitrile) / toluene / 3 h / Heating

3: 570 mg / KOH; H₂O / ethanol / 2 h / Heating

4: K₂CO₃ / acetonitrile; toluene / 18 h / 20 °C

5: 1.34 g / pyridine; DMAP / CH₂Cl₂ / 3 h / 20 °C

With pyridine; dmap; potassium hydroxide; water; tri-n-butyl-tin hydride; potassium carbonate; triethylamine; 1,1'-azobis(1-cyanocyclohexanenitrile); In tetrahydrofuran; ethanol; dichloromethane; toluene; acetonitrile;
DOI:10.1016/S0022-328X(01)00662-3

Reference yield:

: 242130-27-4
(+)-(1R,2R,5S)-N-benzoyloxy-N-methyl-carbamic acid-4,6,6-trimethyl-bicyclo[3.1.1]hept-3-en-2-yl-ester

: 242130-28-5
(+)-(1S,5R,6S)-N-(6-acetoxy-5-isopropyl-2-methyl-cyclohex-2-enyl)-N-methyl-N-(2-prop-2-ynyl)-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / Bu₃SnH; 1,1'-azobis(cyclohexanecarbonitrile) / toluene / 3 h / Heating

2: 570 mg / KOH; H₂O / ethanol / 2 h / Heating

3: K₂CO₃ / acetonitrile; toluene / 18 h / 20 °C

4: 1.34 g / pyridine; DMAP / CH₂Cl₂ / 3 h / 20 °C

With pyridine; dmap; potassium hydroxide; water; tri-n-butyl-tin hydride; potassium carbonate; 1,1'-azobis(1-cyanocyclohexanenitrile); In ethanol; dichloromethane; toluene; acetonitrile;
DOI:10.1016/S0022-328X(01)00662-3

Reference yield:

: 242130-26-3
(+)-(3aS,7R,7aR)-7-isopropyl-3,4-dimethyl-3a,6,7,7a-tetrahydro-3H-benzoxazol-2-one

: 242130-28-5
(+)-(1S,5R,6S)-N-(6-acetoxy-5-isopropyl-2-methyl-cyclohex-2-enyl)-N-methyl-N-(2-prop-2-ynyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 570 mg / KOH; H₂O / ethanol / 2 h / Heating

2: K₂CO₃ / acetonitrile; toluene / 18 h / 20 °C

3: 1.34 g / pyridine; DMAP / CH₂Cl₂ / 3 h / 20 °C

With pyridine; dmap; potassium hydroxide; water; potassium carbonate; In ethanol; dichloromethane; toluene; acetonitrile;
DOI:10.1016/S0022-328X(01)00662-3