Methanesulfonic acid (diethoxy-phosphoryl)-(4-dimethylthiocarbamoyl-phenyl)-methyl ester

Base Information

Chemical Name:Methanesulfonic acid (diethoxy-phosphoryl)-(4-dimethylthiocarbamoyl-phenyl)-methyl ester
CAS No.:134360-23-9
Molecular Formula:C₁₅H₂₄NO₆PS₂
Molecular Weight:409.464
Hs Code.:

Synonyms:Methanesulfonic acid (diethoxy-phosphoryl)-(4-dimethylthiocarbamoyl-phenyl)-methyl ester

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Chemical Property of Methanesulfonic acid (diethoxy-phosphoryl)-(4-dimethylthiocarbamoyl-phenyl)-methyl ester

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Technology Process of Methanesulfonic acid (diethoxy-phosphoryl)-(4-dimethylthiocarbamoyl-phenyl)-methyl ester

There total 2 articles about Methanesulfonic acid (diethoxy-phosphoryl)-(4-dimethylthiocarbamoyl-phenyl)-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 134360-21-7
[(4-Dimethylthiocarbamoyl-phenyl)-hydroxy-methyl]-phosphonic acid diethyl ester

: 124-63-0
methanesulfonyl chloride

: 134360-23-9
Methanesulfonic acid (diethoxy-phosphoryl)-(4-dimethylthiocarbamoyl-phenyl)-methyl ester

Guidance literature:: With triethylamine; In dichloromethane; at -78 ℃;
DOI:10.1021/jo00013a038

Reference yield:

: 134360-17-1
4-(N,N-dimethylthiocarbamoyl)benzaldehyde dimethyl acetal

: 134360-23-9
Methanesulfonic acid (diethoxy-phosphoryl)-(4-dimethylthiocarbamoyl-phenyl)-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / 2percent aq. H₂SO₄ / tetrahydrofuran / 3 h / Ambient temperature

2: 1.) THF, 100 degC, 16 h, 2.) CF₃COOH, room temp., 22.5 h

3: 78 percent / Et₃N / CH₂Cl₂ / -78 °C

With sulfuric acid; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00013a038