2-(3,4-bismethoxymethoxyphenyl)-5-(3-hydroxypropenyl)-7-methoxybenzofuran

Base Information

Chemical Name:2-(3,4-bismethoxymethoxyphenyl)-5-(3-hydroxypropenyl)-7-methoxybenzofuran
CAS No.:1393807-60-7
Molecular Formula:C₂₂H₂₄O₇
Molecular Weight:400.428
Hs Code.:

Synonyms:2-(3,4-bismethoxymethoxyphenyl)-5-(3-hydroxypropenyl)-7-methoxybenzofuran

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Chemical Property of 2-(3,4-bismethoxymethoxyphenyl)-5-(3-hydroxypropenyl)-7-methoxybenzofuran

Chemical Property:

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Technology Process of 2-(3,4-bismethoxymethoxyphenyl)-5-(3-hydroxypropenyl)-7-methoxybenzofuran

There total 4 articles about 2-(3,4-bismethoxymethoxyphenyl)-5-(3-hydroxypropenyl)-7-methoxybenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1393807-55-0
2-(3,4-bismethoxymethoxyphenyl)-5-(carbethoxyethenyl)-7-methoxybenzofuran

: 1393807-60-7
2-(3,4-bismethoxymethoxyphenyl)-5-(3-hydroxypropenyl)-7-methoxybenzofuran

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; at -78 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.5012/bkcs.2012.33.6.1907

Reference yield:

: 5438-36-8
5-iodovaniline

: 1393807-60-7
2-(3,4-bismethoxymethoxyphenyl)-5-(3-hydroxypropenyl)-7-methoxybenzofuran

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 10 h / 20 °C / Inert atmosphere

2: dichloromethane / 8 h / Inert atmosphere; Reflux

3: diisobutylaluminium hydride / tetrahydrofuran / 1.5 h / -78 - 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1: Sonogashira coupling / 2: Wittig-Horner reaction;
DOI:10.5012/bkcs.2012.33.6.1907

Reference yield:

: 1393807-49-2
2-(3,4-bismethoxymethoxyphenyl)-7-methoxybenzofuran-5-carbaldehyde

: 1393807-60-7
2-(3,4-bismethoxymethoxyphenyl)-5-(3-hydroxypropenyl)-7-methoxybenzofuran

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 8 h / Inert atmosphere; Reflux

2: diisobutylaluminium hydride / tetrahydrofuran / 1.5 h / -78 - 20 °C / Inert atmosphere

With diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; 1: Wittig-Horner reaction;
DOI:10.5012/bkcs.2012.33.6.1907