N-[2-(tert-butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethyl]-4-diisopropylaminooxalyl-benzamide

Base Information

Chemical Name:N-[2-(tert-butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethyl]-4-diisopropylaminooxalyl-benzamide
CAS No.:864515-54-8
Molecular Formula:C₃₁H₄₆N₂O₅Si
Molecular Weight:554.802
Hs Code.:

<i>N</i>-[2-(<i>tert</i>-butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethyl]-4-diisopropylaminooxalyl-benzamide

Synonyms:N-[2-(tert-butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethyl]-4-diisopropylaminooxalyl-benzamide

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Chemical Property of N-[2-(tert-butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethyl]-4-diisopropylaminooxalyl-benzamide

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Technology Process of N-[2-(tert-butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethyl]-4-diisopropylaminooxalyl-benzamide

There total 2 articles about N-[2-(tert-butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethyl]-4-diisopropylaminooxalyl-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 864515-64-0
(1S,2S)-2-(tert-Butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethylamine

: 360789-47-5
N,N-bis(1-methylethyl)-α-oxobenzeneacetamide-4-carboxylic acid

: 864515-54-8
N-[2-(tert-butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethyl]-4-diisopropylaminooxalyl-benzamide

Guidance literature:: N,N-bis(1-methylethyl)-α-oxobenzeneacetamide-4-carboxylic acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 0.166667h;

(1S,2S)-2-(tert-Butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/ja043999p

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 864515-54-8
N-[2-(tert-butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethyl]-4-diisopropylaminooxalyl-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 80 percent / 2,6-lutidine / CH₂Cl₂ / cooling

2.1: 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide*HCl / CH₂Cl₂ / 0.17 h / 20 °C

2.2: 75 percent / CH₂Cl₂ / 2 h / 20 °C

With 2,6-dimethylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/ja043999p