Perfluorphenylmethyl-(perfluorphenyl-tributylstannoxymethyl)-ether

Base Information

• Chemical Name: Perfluorphenylmethyl-(perfluorphenyl-tributylstannoxymethyl)-ether
• CAS No.: 20428-47-1
• Molecular Formula: C₂₆H₃₀F₁₀O₂Sn
• Molecular Weight: 683.217
• Mol file: 20428-47-1.mol

Synonyms:Perfluorphenylmethyl-(perfluorphenyl-tributylstannoxymethyl)-ether

Chemical Property of Perfluorphenylmethyl-(perfluorphenyl-tributylstannoxymethyl)-ether

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Perfluorphenylmethyl-(perfluorphenyl-tributylstannoxymethyl)-ether

There total 2 articles about Perfluorphenylmethyl-(perfluorphenyl-tributylstannoxymethyl)-ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

perfluorobenzaldehyde (653-37-2) + tri-n-butyl-tin hydride (688-73-3) → Perfluorphenylmethoxytributylzinn (20749-43-3) + Perfluorphenylmethyl-(perfluorphenyl-tributylstannoxymethyl)-ether (20428-47-1)

Guidance literature:

In neat (no solvent); 2:3 mole ratio of (C4H9)3SnH and aldehyde, 20. degree.C; 2.6:1 mixt. of (C4H9)3SnOCH2C6F5 and the 1:2 adduct (C4H9)3SnOCH(C6F5)OCH2C5F6;

DOI:10.1016/S0022-328X(00)88867-1

Reference yield:

→ Perfluorphenylmethyl-(perfluorphenyl-tributylstannoxymethyl)-ether (20428-47-1)

Guidance literature:

Tributylzinnhydrid, 2,3,4,5,6-Pentafluor-benzaldehyd;

DOI:10.1016/S0022-328X(00)88867-1

Reference yield:

Perfluorphenylmethyl-(perfluorphenyl-tributylstannoxymethyl)-ether (20428-47-1) → Perfluorphenylmethoxytributylzinn (20749-43-3)

Guidance literature:

conversion by distn.;

DOI:10.1016/S0022-328X(00)88867-1

upstream raw materials:

perfluorobenzaldehyde

tri-n-butyl-tin hydride

Downstream raw materials:

Perfluorphenylmethoxytributylzinn