(S)-2-(2-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)-2-hydroxypropoxy)ethyl)-7-methylbenzo[lmn][3 ,8 ]-phenanthroline-1,3,6,8(2H,7H)-tetraone

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Chemical Name:(S)-2-(2-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)-2-hydroxypropoxy)ethyl)-7-methylbenzo[lmn][3 ,8 ]-phenanthroline-1,3,6,8(2H,7H)-tetraone
CAS No.:1566613-79-3
Molecular Formula:C₄₁H₃₆N₂O₉
Molecular Weight:700.745
Hs Code.:

Synonyms:(S)-2-(2-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)-2-hydroxypropoxy)ethyl)-7-methylbenzo[lmn][3 ,8 ]-phenanthroline-1,3,6,8(2H,7H)-tetraone

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Chemical Property of (S)-2-(2-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)-2-hydroxypropoxy)ethyl)-7-methylbenzo[lmn][3 ,8 ]-phenanthroline-1,3,6,8(2H,7H)-tetraone

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Technology Process of (S)-2-(2-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)-2-hydroxypropoxy)ethyl)-7-methylbenzo[lmn][3 ,8 ]-phenanthroline-1,3,6,8(2H,7H)-tetraone

There total 3 articles about (S)-2-(2-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)-2-hydroxypropoxy)ethyl)-7-methylbenzo[lmn][3 ,8 ]-phenanthroline-1,3,6,8(2H,7H)-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52705-06-3
2-methyl-1,3-dioxo-2,3-dihydro-1H-benzo[de]isoquinoline-6,7-dicarboxylic acid anhydride

: 1566613-76-0
(S)-1-(2-aminoethoxy)-3-(bis(4-methoxyphenyl)(phenyl)methoxy)propan-2-ol

: 1566613-79-3
(S)-2-(2-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)-2-hydroxypropoxy)ethyl)-7-methylbenzo[lmn][3 ,8 ]-phenanthroline-1,3,6,8(2H,7H)-tetraone

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 140 ℃; for 0.0833333h; Microwave irradiation;
DOI:10.1021/jo402704z

Reference yield:

: 1566613-73-7
(R)-2-(2-(2,3-dihydroxypropoxy)ethyl)isoindoline-1,3-dione

: 1566613-79-3
(S)-2-(2-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)-2-hydroxypropoxy)ethyl)-7-methylbenzo[lmn][3 ,8 ]-phenanthroline-1,3,6,8(2H,7H)-tetraone

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 4 h / 20 °C / Inert atmosphere

2: methylamine / ethanol / 2.5 h / 78 °C / Inert atmosphere

3: triethylamine / N,N-dimethyl-formamide / 0.08 h / 140 °C / Microwave irradiation

With pyridine; triethylamine; methylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo402704z

Reference yield:

: 1566613-74-8
(S)-2-(2-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)-2-hydroxypropoxy)ethyl)isoindoline-1,3-dione

: 1566613-79-3
(S)-2-(2-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)-2-hydroxypropoxy)ethyl)-7-methylbenzo[lmn][3 ,8 ]-phenanthroline-1,3,6,8(2H,7H)-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1: methylamine / ethanol / 2.5 h / 78 °C / Inert atmosphere

2: triethylamine / N,N-dimethyl-formamide / 0.08 h / 140 °C / Microwave irradiation

With triethylamine; methylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo402704z