benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-7-hydroxy-2-methyl-3-heptylcarbamate

Base Information

Chemical Name:benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-7-hydroxy-2-methyl-3-heptylcarbamate
CAS No.:1227183-22-3
Molecular Formula:C₂₅H₄₆N₂O₄Si
Molecular Weight:466.737
Hs Code.:

Synonyms:benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-7-hydroxy-2-methyl-3-heptylcarbamate

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Chemical Property of benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-7-hydroxy-2-methyl-3-heptylcarbamate

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Technology Process of benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-7-hydroxy-2-methyl-3-heptylcarbamate

There total 1 articles about benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-7-hydroxy-2-methyl-3-heptylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1227182-97-9
benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate

: 1227183-22-3
benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-7-hydroxy-2-methyl-3-heptylcarbamate

Guidance literature:: benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1007/s00706-009-0239-y

Reference yield: 32.0%

: 1227183-22-3
benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-7-hydroxy-2-methyl-3-heptylcarbamate

: 1242316-68-2
(5S,1'S,2''S)-5-(1-benzyloxycarbonylamino-3-methylpropyl)-1-(1-tert-butyldimethylsilyloxypropan-2-yl)pyrrolidin-2-one

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 3h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2010.05.099