benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate

Base Information

Chemical Name:benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate
CAS No.:1227182-97-9
Molecular Formula:C₂₅H₄₄N₂O₃Si
Molecular Weight:448.721
Hs Code.:

Synonyms:benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate

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Chemical Property of benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate

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Technology Process of benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate

There total 1 articles about benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: C₂₂H₃₈N₂O₃Si

: 106-95-6
allyl bromide

: 1227182-98-0
benzyl (3S,4R,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate

: 1227182-97-9
benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate

Guidance literature:: allyl bromide; With cerium(III) chloride heptahydrate; zinc; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

C₂₂H₃₈N₂O₃Si; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1007/s00706-009-0239-y

Reference yield: 89.0%

: 1227182-97-9
benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate

: 1227183-22-3
benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-7-hydroxy-2-methyl-3-heptylcarbamate

Guidance literature:: benzyl (3S,4S,2'S)-4-[1-(tert-butyldimethylsilyloxy)-2-propylamino]-2-methylhept-6-en-3-ylcarbamate; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1007/s00706-009-0239-y