1-METHYL-4-PHENYL-BUTYLAMINE

Base Information

Chemical Name:1-METHYL-4-PHENYL-BUTYLAMINE
CAS No.:22148-82-9
Molecular Formula:C₁₁H₁₇N
Molecular Weight:163.263
Hs Code.:2921499090
Mol file:22148-82-9.mol

Synonyms:Benzenebutanamine, a-methyl-, (?à)-; Butylamine, 1-methyl-4-phenyl-, (?à)- (8CI)

Suppliers and Price of 1-METHYL-4-PHENYL-BUTYLAMINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
1-Methyl-4-phenyl-butylamine
1g
$ 485.00

Matrix Scientific
1-Methyl-4-phenyl-butylamine
500mg
$ 315.00

Crysdot
5-Phenylpentan-2-amine 95+%
5g
$ 874.00

American Custom Chemicals Corporation
1-METHYL-4-PHENYL-BUTYLAMINE 95.00%
500MG
$ 777.32

AK Scientific
1-Methyl-4-phenyl-butylamine
1g
$ 704.00

Total 7 raw suppliers

Chemical Property of 1-METHYL-4-PHENYL-BUTYLAMINE

Chemical Property:

Boiling Point:259.2 °C at 760 mmHg
Flash Point:108.7 °C
PSA：26.02000
Density:0.928g/cm³
LogP:3.05680

Purity/Quality:

98%min ^*data from raw suppliers

1-Methyl-4-phenyl-butylamine ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-METHYL-4-PHENYL-BUTYLAMINE

There total 8 articles about 1-METHYL-4-PHENYL-BUTYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42762-51-6
(E)-5-phenyl-3-penten-2-one

: 22148-82-9,72456-67-8
5-phenylpentan-2-amine

Guidance literature:: With palladium 10% on activated carbon; ammonia; hydrogen; In methanol; at 20 ℃; under 6000.6 Torr;
DOI:10.1055/s-0029-1218672

Reference yield:

: 377080-79-0
(4R,1'R)-3-(1'-methyl-4'-phenylbutyl)-4-phenyloxazolidin-2-one

: 22148-82-9,72456-67-8,72457-54-6
(S)-2-amino-5-phenylpentane

: (R)-2-amino-5-phenylpentane

Guidance literature:: With ammonia; lithium; In tetrahydrofuran; at -78 ℃; for 0.333333h; Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(01)00323-8

Reference yield:

: 22818-69-5
(3-nitropropyl)benzene

: 22148-82-9,72456-67-8,72457-54-6
(S)-2-amino-5-phenylpentane

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / methanol / 0.33 h / 0 °C

1.2: methanol / 48 h / 20 °C

2.1: 48 percent / 4-(N,N-dimethylamino)pyridine; acetic anhydride / diethyl ether / 20 °C

3.1: 69 percent / 18-crown-6 / tetrahydrofuran / 0.5 h / -78 °C

4.1: 79 percent / α,α'-azobisisobutyronitrile; tributyltin hydride / toluene / 2 h / Heating

5.1: lithium; liq. ammonia / tetrahydrofuran / 0.33 h / -78 °C

With dmap; potassium hydroxide; 18-crown-6 ether; azobisisobutyronitrile; ammonia; tri-n-butyl-tin hydride; acetic anhydride; lithium; In tetrahydrofuran; methanol; diethyl ether; toluene; 5.1: Birch reduction;
DOI:10.1016/S0957-4166(01)00323-8